1-Butanol, 4-(ethenyloxy)-

Base Information

• Chemical Name: 1-Butanol, 4-(ethenyloxy)-
• CAS No.: 17832-28-9
• Molecular Formula: C6H12O2
• Molecular Weight: 116.16
• Hs Code.: 2909 49 80
• European Community (EC) Number: 241-793-5
• UNII: 8LGM5RZX0N
• DSSTox Substance ID: DTXSID6044854
• Nikkaji Number: J51.553A
• Wikidata: Q27270719
• RXCUI: 2289429
• ChEMBL ID: CHEMBL3182123
• Mol file: 17832-28-9.mol

Synonyms:17832-28-9;4-(Vinyloxy)butan-1-ol;1-Butanol, 4-(ethenyloxy)-;1,4-Butanediol vinyl ether;4-Hydroxybutyl vinyl ether;4-(Ethenyloxy)butan-1-ol;4-ethenoxybutan-1-ol;hydroxybutyl vinyl ether;UNII-8LGM5RZX0N;8LGM5RZX0N;4-(Vinyloxy)-1-butanol;DTXSID6044854;EINECS 241-793-5;EC 241-793-5;1,4-Butanediol monovinyl ether;4-Vinyloxybutanol;31244-41-4;(Ethenyloxy)-butanol;HBUVE;HBVE;Hydroxybutyvinyl ether;4-vinyloxy-1-butanol;RAPI-CURE HBVE;4-vinyloxy-butan-1-ol;4-hydroxybutylvinyl ether;4-(ethenyloxy)-1-butanol;4-(VINYLOXY)BUTANOL;SCHEMBL36631;SCHEMBL4287931;4-ETHENYLOXY-1-BUTANOL;CHEMBL3182123;DTXCID4024854;butane-1,4-diol;vinyloxyethylene;Tox21_301676;1-BUTANOL, 4-(VINYLOXY)-;MFCD00080697;AKOS015915491;NCGC00256071-01;CAS-17832-28-9;CS-0077087;FT-0637609;T1796;E81009;EN300-7465856;A812358;Q27270719;1,4-Butanediol vinyl ether, contains 0.01% potassium hydroxide as stabilizer, 99%

Chemical Property of 1-Butanol, 4-(ethenyloxy)-

Chemical Property:

• Appearance/Colour: colorless to yellow liquid
• Vapor Pressure: 0.00263mmHg at 25°C
• Melting Point: -33 °C
• Refractive Index: n20/D 1.444(lit.)
• Boiling Point: 181.5 °C at 760 mmHg
• PKA: 15.04±0.10(Predicted)
• Flash Point: 67.9 °C
• PSA: 29.46000
• Density: 0.917 g/cm³
• LogP: 0.91900
• Storage Temp.: Store at
• Solubility.: 75g/l
• Water Solubility.: 75 g/L (20 ºC)
• XLogP3: 0.9
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 5
• Exact Mass: 116.083729621
• Heavy Atom Count: 8
• Complexity: 52.5

Purity/Quality:

99% ^*data from raw suppliers

1,4-Butanediol vinyl ether ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xn
• Hazard Codes: Xn
• Statements: 20/21/22-36/37/38-22-52/53
• Safety Statements: 26-36-24/25-61

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: C=COCCCCO

Technology Process of 1-Butanol, 4-(ethenyloxy)-

There total 4 articles about 1-Butanol, 4-(ethenyloxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

2-phenylsulfonylmethyl-1,3-dioxepane (425429-11-4) → 4-(vinyloxy)butan-1-ol (17832-28-9)

Guidance literature:

With sodium dihydrogenphosphate; sodium amalgam; In methanol; at 20 ℃;

DOI:10.1016/S0040-4039(01)02195-5

Reference yield: 48.0%

Butane-1,4-diol (110-63-4) + acetylene (74-86-2,25067-58-7) → 4-(vinyloxy)butan-1-ol (17832-28-9) + 1,4-divinyloxybutane (3891-33-6,164978-32-9)

Guidance literature:

With sodium hydroxide; cesium fluoride; at 138 - 140 ℃; for 2h; under 7355.08 - 8826.1 Torr;

DOI:10.1007/s11178-005-0223-x

Reference yield:

Butane-1,4-diol (110-63-4) + acetylene (74-86-2,25067-58-7) → 4-(vinyloxy)butan-1-ol (17832-28-9)

Guidance literature:

With potassium hydroxide; at 130 - 150 ℃; under 14710.2 - 25742.8 Torr;

upstream raw materials:

Butane-1,4-diol

acetylene

2-phenylsulfonylmethyl-1,3-dioxepane

Downstream raw materials:

2-methyl-[1,3]dioxepane

-butyl vinyl ether

Butane-1,4-diol

4-(vinyloxy)butyl 4-methylbenzenesulfonate

Refernces

Synthesis and photopolymerization of bifunctional liquid crystalline vinyl ether monomers

10.1080/10587259408037773

The research focuses on the synthesis and photopolymerization of bifunctional liquid crystalline vinyl ether monomers, with the purpose of creating highly ordered, densely crosslinked liquid crystalline poly(viny1 ether) films. The study aimed to explore the potential of these materials in optical, electrical, and mechanical applications by achieving orientation through a simple surface treatment using a unidirectionally rubbed polyimide film. The researchers synthesized and polymerized two different monomers, resulting in liquid crystalline polymer (LC polymer) network films with varying molecular organizations, including nematic, smectic A, and smectic B structures. The chemicals used in the process included phenacyltetramethylenesulfonium hexafluoroantimonate as a photoinitiator, phenothazine as a photosensitizer, 4-[11-(vinyloxy)undecyloxy]benzoic acid, 2-hydroxyethyl vinyl ether, 4-hydroxybutyl vinyl ether, and 1,3-dicyclohexylcarbodiimide, among others. The conclusions of the research indicated that by in situ photopolymerization of these bifunctional mesogenic vinyl ether monomers with various mesophases, it was possible to prepare LC polymer networks with different molecular structures, demonstrating the potential for tailored materials with specific properties for various applications.

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