8-METHOXY-2-METHYLQUINOLINE

Base Information

• Chemical Name: 8-METHOXY-2-METHYLQUINOLINE
• CAS No.: 3033-80-5
• Molecular Formula: C11H11 N O
• Molecular Weight: 173.214
• Hs Code.: 2933499090
• Mol file: 3033-80-5.mol

Synonyms:Quinaldine,8-methoxy- (6CI,7CI,8CI); 2-Methyl-8-methoxyquinoline;8-Methoxy-2-methylquinoline; 8-Methoxyquinaldine; NSC 246071

Chemical Property of 8-METHOXY-2-METHYLQUINOLINE

Chemical Property:

• Vapor Pressure: 0.00467mmHg at 25°C
• Melting Point: 124°C
• Boiling Point: 286°Cat760mmHg
• PKA: 4.13±0.50(Predicted)
• Flash Point: 104.9°C
• PSA: 22.12000
• Density: 1.102g/cm³
• LogP: 2.55180

Purity/Quality:

99%, ^*data from raw suppliers

8-methoxy-2-methylquinoline ^*data from reagent suppliers

Safty Information:

• Statements: 36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of 8-METHOXY-2-METHYLQUINOLINE

There total 4 articles about 8-METHOXY-2-METHYLQUINOLINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

(E)-4-(3-methoxyphenyl)butan-2-one oxime (191484-58-9) → 8-methoxy-2-methylquinoline (3033-80-5) + 6-methoxyquinaldine (1078-28-0)

Guidance literature:

With chloranil; trifluoroacetic anhydride; In dichloromethane; at 20 ℃; for 22h;

DOI:10.1055/s-2003-42439

Reference yield: 81.0%

4-(3-methoxyphenyl)butan-2-one (Z)-oxime → 8-methoxy-2-methylquinoline (3033-80-5) + 6-methoxyquinaldine (1078-28-0)

Guidance literature:

With chloranil; trifluoroacetic anhydride; In dichloromethane; at 20 ℃; for 22h;

DOI:10.1055/s-2003-42439

Reference yield: 15.0%

4-(3-methoxyphenyl)-2-butanone oxime (79204-83-4) → 8-methoxy-2-methylquinoline (3033-80-5) + 6-methoxyquinaldine (1078-28-0)

Guidance literature:

With trifluorormethanesulfonic acid; 5A molecular sieve; chloranil; tetrabutylammonium perrhenate; In dichloromethane; for 2h; Heating;

DOI:10.1246/cl.1995.5

upstream raw materials:

4-(3-methoxyphenyl)-2-butanone oxime

(E)-4-(3-methoxyphenyl)butan-2-one oxime

2-methoxy-phenylamine

ethyl vinyl ether

Downstream raw materials:

8-methoxyquinoline-2-carboxylic acid

8-hydroxy-quinoline-2-carboxylic acid

5,7-dibromo-2-methylquinolin-8-ol

3-((8-methoxyquinolin-2-yl)methyl)-2-tosylisoindolin-1-one

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