1,3-Dioxolane, 2-[3-nitro-4-phenyl-3-(phenylmethyl)-1-butenyl]-, (E)-

Base Information

Chemical Name:1,3-Dioxolane, 2-[3-nitro-4-phenyl-3-(phenylmethyl)-1-butenyl]-, (E)-
CAS No.:114090-52-7
Molecular Formula:C₂₀H₂₁NO₄
Molecular Weight:339.391
Hs Code.:

Synonyms:

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Chemical Property of 1,3-Dioxolane, 2-[3-nitro-4-phenyl-3-(phenylmethyl)-1-butenyl]-, (E)-

Chemical Property:

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Technology Process of 1,3-Dioxolane, 2-[3-nitro-4-phenyl-3-(phenylmethyl)-1-butenyl]-, (E)-

There total 7 articles about 1,3-Dioxolane, 2-[3-nitro-4-phenyl-3-(phenylmethyl)-1-butenyl]-, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 107-21-1
ethylene glycol

: 114090-51-6
(E)-4-benzyl-4-nitro-5-phenylpent-2-enal

: 114090-52-7
(E)-4-benzyl-4-nitro-5-phenylpent-2-enal ethylene acetal

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 17h; Heating;
DOI:10.1039/P19870002027

Reference yield:

: 6125-24-2
2-Phenylnitroethane

: 114090-52-7
(E)-4-benzyl-4-nitro-5-phenylpent-2-enal ethylene acetal

Guidance literature:: Multi-step reaction with 6 steps

1: MeNH₂*HCl, AcOK, trimethyl orthoformate / methanol / 16 h / Heating

2: NaBH₄ / dimethylsulfoxide / 1 h / 20 °C

3: 71 percent / tetra-n-butylammonium chloride, KF*2H₂O / dimethylformamide / 4 h

4: 79 percent / 25percent di-isobutylaluminium hydride / toluene / 3 h / 0 °C

5: 76 percent / MnO₂ / CH₂Cl₂ / 0.25 h

6: 81 percent / toluene-p-sulphonic acid monohydrate / benzene / 17 h / Heating

With manganese(IV) oxide; potassium fluoride; sodium tetrahydroborate; diisobutylaluminum hydride; tetrabutyl-ammonium chloride; methylamine hydrochloride; potassium acetate; toluene-4-sulfonic acid; trimethyl orthoformate; In methanol; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; benzene;
DOI:10.1039/P19870002027

Reference yield:

: 58497-32-8
(2-nitroprop-1-ene-1,3-diyl)dibenzene

: 114090-52-7
(E)-4-benzyl-4-nitro-5-phenylpent-2-enal ethylene acetal

Guidance literature:: Multi-step reaction with 5 steps

1: NaBH₄ / dimethylsulfoxide / 1 h / 20 °C

2: 71 percent / tetra-n-butylammonium chloride, KF*2H₂O / dimethylformamide / 4 h

3: 79 percent / 25percent di-isobutylaluminium hydride / toluene / 3 h / 0 °C

4: 76 percent / MnO₂ / CH₂Cl₂ / 0.25 h

5: 81 percent / toluene-p-sulphonic acid monohydrate / benzene / 17 h / Heating

With manganese(IV) oxide; potassium fluoride; sodium tetrahydroborate; diisobutylaluminum hydride; tetrabutyl-ammonium chloride; toluene-4-sulfonic acid; In dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; benzene;
DOI:10.1039/P19870002027