(3,5-Dibromo-4-methoxyphenyl)methanol

Base Information

Chemical Name:(3,5-Dibromo-4-methoxyphenyl)methanol
CAS No.:114113-99-4
Molecular Formula:C8H8Br2O2
Molecular Weight:295.958
Hs Code.:
European Community (EC) Number:817-269-2
DSSTox Substance ID:DTXSID80579688
Wikidata:Q82470295
Mol file:114113-99-4.mol

Synonyms:(3,5-Dibromo-4-methoxyphenyl)methanol;114113-99-4;Benzenemethanol, 3,5-dibromo-4-methoxy-;DTXSID80579688;MFCD12047705;3,5-dibromo-4-methoxy benzyl alcohol;AB93341;CS-0194610;E90705;EN300-365355

Suppliers and Price of (3,5-Dibromo-4-methoxyphenyl)methanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of (3,5-Dibromo-4-methoxyphenyl)methanol

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:295.88706
Heavy Atom Count:12
Complexity:131

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1Br)CO)Br

Technology Process of (3,5-Dibromo-4-methoxyphenyl)methanol

There total 3 articles about (3,5-Dibromo-4-methoxyphenyl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 108940-96-1
3,5-dibromo-4-methoxybenzaldehyde

: 114113-99-4
(3,5-dibromo-4-methoxyphenyl)methanol

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 20 ℃; for 2h;
DOI:10.1021/ol0510062

Reference yield:

: 2973-77-5
3,5-dibromo-4-hydroxybenzaldehyde

: 114113-99-4
(3,5-dibromo-4-methoxyphenyl)methanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 55 °C

2.1: sodium tetrahydroborate / ethanol / 5 h / 0 - 20 °C

2.2: 20 °C

With sodium tetrahydroborate; potassium carbonate; In ethanol; N,N-dimethyl-formamide; 1.1: Williamson synthesis;
DOI:10.1016/j.tet.2011.10.021