3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-, methyl 3-[4-[2-[(tetrahydro-2H-pyran-2-yl)oxy]ethyl]phenoxy]propyl ester, (4R)-

Base Information

• Chemical Name: 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-, methyl 3-[4-[2-[(tetrahydro-2H-pyran-2-yl)oxy]ethyl]phenoxy]propyl ester, (4R)-
• CAS No.: 114207-82-8
• Molecular Formula: C₃₂H₃₈N₂O₉
• Molecular Weight: 594.662
• Mol file: 114207-82-8.mol

Synonyms:

Chemical Property of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-, methyl 3-[4-[2-[(tetrahydro-2H-pyran-2-yl)oxy]ethyl]phenoxy]propyl ester, (4R)-

Chemical Property:

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Useful:

Technology Process of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-, methyl 3-[4-[2-[(tetrahydro-2H-pyran-2-yl)oxy]ethyl]phenoxy]propyl ester, (4R)-

There total 3 articles about 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-, methyl 3-[4-[2-[(tetrahydro-2H-pyran-2-yl)oxy]ethyl]phenoxy]propyl ester, (4R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-(4-[2-(tetrahydropyran-2-yloxy)ethyl]phenoxy)propyl acetoacetate + 3-nitro-benzaldehyde (99-61-6) + methyl 3-aminocrotonate (21731-17-9) → (S,RS)-2,6-dimethyl-3-carbomethoxy-4-(3-nitrophenyl)-5-[3-(4-[2-(tetrahydropyran-2-yloxy)ethyl]phenoxy)propoxycarbonyl]-1,4-dihydropyridine (114207-71-5,114207-76-0,114207-82-8)

Guidance literature:

In ethanol;

Reference yield:

2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydropyridine-3,5-dicarboxylic acid 3-methyl ester 5-(3-bromopropyl)-ester (114208-20-7,114208-21-8,114208-22-9) + potassium carbonate (584-08-7) + 4-{2-[(tetrahydro-2H-pyran-2-yl)oxy]ethyl}phenol (114208-16-1) → (S,RS)-2,6-dimethyl-3-carbomethoxy-4-(3-nitrophenyl)-5-[3-(4-[2-(tetrahydropyran-2-yloxy)ethyl]phenoxy)propoxycarbonyl]-1,4-dihydropyridine (114207-71-5,114207-76-0,114207-82-8) + 2,6-dimethyl-3-carbomethoxy-4-(3-nitrophenyl)-5-(3-[4-(2-tetrahydropyran-2-yloxyethyl)phenyl]propoxycarbonyl)-1,4-dihydropyridine

Guidance literature:

In dichloromethane; acetone;

Reference yield:

→ (S,RS)-2,6-dimethyl-3-carbomethoxy-4-(3-nitrophenyl)-5-[3-(4-[2-(tetrahydropyran-2-yloxy)ethyl]phenoxy)propoxycarbonyl]-1,4-dihydropyridine (114207-71-5,114207-76-0,114207-82-8)

Guidance literature:

upstream raw materials:

3-nitro-benzaldehyde

methyl 3-aminocrotonate

2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydropyridine-3,5-dicarboxylic acid 3-methyl ester 5-(3-bromopropyl)-ester

potassium carbonate

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