Technology Process of Tetraphenylgermane
There total 42 articles about Tetraphenylgermane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
phenylmagnesium bromide;
In
diethyl ether;
(N2); added dropwise C6H5MgBr to a suspn. of Ge-compound at room temp.; stirred for 15 min; hydrolyzed; pptd.; filtered; extracted with CHCl3; washed with water; dried over MgSO4; evapd.; recrystd. from toluene;
DOI:10.1021/om00051a049
- Guidance literature:
-
With
phenylmagnesium bromide;
In
diethyl ether;
(N2); added dropwise C6H5MgBr to a suspn. of Ge-compound at room temp.; stirred for 15 min; hydrolyzed; pptd.; filtered; extracted with CHCl3; washed with water; dried over MgSO4; evapd.; recrystd. from toluene;
DOI:10.1021/om00051a049
- Guidance literature:
-
bromobenzene;
With
magnesium;
In
tetrahydrofuran;
germaniumtetrachloride;
In
tetrahydrofuran;
for 18h;
Reflux;
DOI:10.1002/chem.201505084
Xn
