3-Bromo-N-[2-(3-bromo-4-hydroxyphenyl)ethyl]-5-[2,6-dibromo-4-[3-[[2-(3-bromo-4-hydroxyphenyl)ethyl]amino]-2-(hydroxyimino)-3-oxopropyl]phenoxy]-4-hydroxy-α-(hydroxyimino)benzenepropanamide

Base Information

Chemical Name:3-Bromo-N-[2-(3-bromo-4-hydroxyphenyl)ethyl]-5-[2,6-dibromo-4-[3-[[2-(3-bromo-4-hydroxyphenyl)ethyl]amino]-2-(hydroxyimino)-3-oxopropyl]phenoxy]-4-hydroxy-α-(hydroxyimino)benzenepropanamide
CAS No.:75513-47-2
Molecular Formula:C34H29Br5N4O8
Molecular Weight:1021.13606
Hs Code.:
Mol file:75513-47-2.mol

3-Bromo-N-[2-(3-bromo-4-hydroxyphenyl)ethyl]-5-[2,6-dibromo-4-[3-[[2-(3-bromo-4-hydroxyphenyl)ethyl]amino]-2-(hydroxyimino)-3-oxopropyl]phenoxy]-4-hydroxy-α-(hydroxyimino)benzenepropanamide

Synonyms:

Suppliers and Price of 3-Bromo-N-[2-(3-bromo-4-hydroxyphenyl)ethyl]-5-[2,6-dibromo-4-[3-[[2-(3-bromo-4-hydroxyphenyl)ethyl]amino]-2-(hydroxyimino)-3-oxopropyl]phenoxy]-4-hydroxy-α-(hydroxyimino)benzenepropanamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-Bromo-N-[2-(3-bromo-4-hydroxyphenyl)ethyl]-5-[2,6-dibromo-4-[3-[[2-(3-bromo-4-hydroxyphenyl)ethyl]amino]-2-(hydroxyimino)-3-oxopropyl]phenoxy]-4-hydroxy-α-(hydroxyimino)benzenepropanamide

Chemical Property:

PSA：193.30000
LogP:8.65320

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Bromo-N-[2-(3-bromo-4-hydroxyphenyl)ethyl]-5-[2,6-dibromo-4-[3-[[2-(3-bromo-4-hydroxyphenyl)ethyl]amino]-2-(hydroxyimino)-3-oxopropyl]phenoxy]-4-hydroxy-α-(hydroxyimino)benzenepropanamide

There total 11 articles about 3-Bromo-N-[2-(3-bromo-4-hydroxyphenyl)ethyl]-5-[2,6-dibromo-4-[3-[[2-(3-bromo-4-hydroxyphenyl)ethyl]amino]-2-(hydroxyimino)-3-oxopropyl]phenoxy]-4-hydroxy-α-(hydroxyimino)benzenepropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 83047-64-7
bis-p-methoxybenzyl bastadin-2

: 75513-47-2
prebastadin 2

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 0.333333h; Ambient temperature;
DOI:10.1016/S0040-4039(00)87083-5

Reference yield: 68.0%

: 98489-01-1
2-(3-bromo-4-hydroxyphenyl)ethylamine

: 3-[3,5-Dibromo-4-(3-bromo-5-{2-carboxy-2-[(E)-hydroxyimino]-ethyl}-2-hydroxy-phenoxy)-phenyl]-2-[(E)-hydroxyimino]-propionic acid

: 75513-47-2
3-[3-Bromo-5-(2,6-dibromo-4-{2-[2-(3-bromo-4-hydroxy-phenyl)-ethylcarbamoyl]-2-[(Z)-hydroxyimino]-ethyl}-phenoxy)-4-hydroxy-phenyl]-N-[2-(3-bromo-4-hydroxy-phenyl)-ethyl]-2-[(E)-hydroxyimino]-propionamide

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; at 24 ℃; for 24h;
DOI:10.1021/jo9721204

Reference yield:

: 2973-78-6
3-bromo-4-hydroxybenzylaldehyde

: 75513-47-2
prebastadin 2

Guidance literature:: Multi-step reaction with 7 steps

2: K₂CO₃ / tetrahydrofuran / 18 h / Ambient temperature

3: 79 percent / Ac₂O, pyridine

4: 65 percent / NaBH₄ / bis-(2-methoxy-ethyl) ether / 1 h / 0 °C

5: Zn, AcOH / dioxane / 0.67 h / 0 - 5 °C

6: 36 percent / 36 h / 65 °C

7: 82 percent / trifluoroacetic acid / CH₂Cl₂ / 0.33 h / Ambient temperature

With pyridine; sodium tetrahydroborate; acetic anhydride; potassium carbonate; acetic acid; trifluoroacetic acid; zinc; In tetrahydrofuran; 1,4-dioxane; dichloromethane; diethylene glycol dimethyl ether;
DOI:10.1016/S0040-4039(00)87083-5