1,3-Benzenedimethanol,5-(1,1-dimethylethyl)-a1,a1,a3,a3-tetramethyl-2-(methylthio)-

Base Information

• Chemical Name: 1,3-Benzenedimethanol,5-(1,1-dimethylethyl)-a1,a1,a3,a3-tetramethyl-2-(methylthio)-
• CAS No.: 64407-85-8
• Molecular Formula: C₁₇H₂₈O₂S
• Molecular Weight: 296.474

Synonyms:1,3-Benzenedimethanol,5-(1,1-dimethylethyl)-a,a,a',a'-tetramethyl-2-(methylthio)- (9CI); NSC 312838

Chemical Property of 1,3-Benzenedimethanol,5-(1,1-dimethylethyl)-a1,a1,a3,a3-tetramethyl-2-(methylthio)-

Chemical Property:

• Boiling Point: 359.9°Cat760mmHg
• Flash Point: 175°C
• Density: 1.06g/cm³

Purity/Quality:

99.5% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3-Benzenedimethanol,5-(1,1-dimethylethyl)-a1,a1,a3,a3-tetramethyl-2-(methylthio)-

There total 1 articles about 1,3-Benzenedimethanol,5-(1,1-dimethylethyl)-a1,a1,a3,a3-tetramethyl-2-(methylthio)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.7%

methylmagnesium bromide (75-16-1) + 7,7'-dicarbethoxy-5,5'-bis(1,1-dimethylethyl)-3,3,3',3'-tetramethyl-1,1'-spiro<3H-2,1-benzoxathiole> 1-oxide (75894-03-0) → 2-(5-tert-Butyl-3,3-dimethyl-1-oxo-1,3-dihydro-1λ4-benzo[c][1,2]oxathiol-7-yl)-propan-2-ol (69105-30-2) + 1-bis(1-hydroxy-1-methylethyl)-5-(1,1-dimethylethyl)benzene (75894-05-2) + 2-[5-tert-Butyl-3-(1-hydroxy-1-methyl-ethyl)-2-methylsulfanyl-phenyl]-propan-2-ol (64407-85-8) + 7,7'-bis(1-hydroxy-1-methylethyl)-5,5'-bis(1,1-dimethylethyl)-3,3,3',3'-tetramethyl-1,1'-spiro<3H-2,1-benzoxathiole> 1-oxide (75894-04-1)

Guidance literature:

In diethyl ether; for 3h;

DOI:10.1021/ja00391a023

upstream raw materials:

methylmagnesium bromide

7,7'-dicarbethoxy-5,5'-bis(1,1-dimethylethyl)-3,3,3',3'-tetramethyl-1,1'-spiro<3H-2,1-benzoxathiole> 1-oxide

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