Bicyclo[2.2.1]heptane-2-acetic acid, 2-hydroxy-1,7,7-trimethyl-a-phenyl-, 2-(dimethylamino)ethyl ester, hydrochloride

Base Information

• Chemical Name: Bicyclo[2.2.1]heptane-2-acetic acid, 2-hydroxy-1,7,7-trimethyl-a-phenyl-, 2-(dimethylamino)ethyl ester, hydrochloride
• CAS No.: 114493-95-7
• Molecular Formula: C₂₂H₃₃NO₃*ClH
• Molecular Weight: 395.97
• Mol file: 114493-95-7.mol

Synonyms:

Chemical Property of Bicyclo[2.2.1]heptane-2-acetic acid, 2-hydroxy-1,7,7-trimethyl-a-phenyl-, 2-(dimethylamino)ethyl ester, hydrochloride

Chemical Property:

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Bicyclo[2.2.1]heptane-2-acetic acid, 2-hydroxy-1,7,7-trimethyl-a-phenyl-, 2-(dimethylamino)ethyl ester, hydrochloride

There total 4 articles about Bicyclo[2.2.1]heptane-2-acetic acid, 2-hydroxy-1,7,7-trimethyl-a-phenyl-, 2-(dimethylamino)ethyl ester, hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

(2-chloroethyl)dimethylamine hydrochloride (4584-46-7) + ((1R,2R,4R)-2-Hydroxy-1,7,7-trimethyl-bicyclo[2.2.1]hept-2-yl)-phenyl-acetic acid (85170-71-4,85170-72-5,85170-77-0,85170-78-1,94063-40-8,94063-41-9,94063-44-2,94063-45-3) → ((1R,2R,4R)-2-Hydroxy-1,7,7-trimethyl-bicyclo[2.2.1]hept-2-yl)-phenyl-acetic acid 2-dimethylamino-ethyl ester; hydrochloride (94013-38-4,94013-40-8,94013-51-1,94013-53-3,94063-27-1,94063-28-2,94063-36-2,94063-38-4,114493-95-7)

Guidance literature:

With sodium isopropylate; In isopropyl alcohol; for 36h; Heating;

DOI:10.1002/ardp.19843171114

Reference yield: 50.0%

(2-chloroethyl)dimethylamine hydrochloride (4584-46-7) + ((1S,2S,4S)-2-Hydroxy-1,7,7-trimethyl-bicyclo[2.2.1]hept-2-yl)-phenyl-acetic acid (85170-71-4,85170-72-5,85170-77-0,85170-78-1,94063-40-8,94063-41-9,94063-44-2,94063-45-3) → ((1S,2S,4S)-2-Hydroxy-1,7,7-trimethyl-bicyclo[2.2.1]hept-2-yl)-phenyl-acetic acid 2-dimethylamino-ethyl ester; hydrochloride (94013-38-4,94013-40-8,94013-51-1,94013-53-3,94063-27-1,94063-28-2,94063-36-2,94063-38-4,114493-95-7)

Guidance literature:

With sodium isopropylate; In isopropyl alcohol; for 36h; Heating;

DOI:10.1002/ardp.19843171114

Reference yield: 42.0%

(2-chloroethyl)dimethylamine hydrochloride (4584-46-7) + ((1R,2S,4R)-2-Hydroxy-1,7,7-trimethyl-bicyclo[2.2.1]hept-2-yl)-phenyl-acetic acid (85170-71-4,85170-72-5,85170-77-0,85170-78-1,94063-40-8,94063-41-9,94063-44-2,94063-45-3) → ((1R,2S,4R)-2-Hydroxy-1,7,7-trimethyl-bicyclo[2.2.1]hept-2-yl)-phenyl-acetic acid 2-dimethylamino-ethyl ester; hydrochloride (94013-38-4,94013-40-8,94013-51-1,94013-53-3,94063-27-1,94063-28-2,94063-36-2,94063-38-4,114493-95-7)

Guidance literature:

With sodium isopropylate; In isopropyl alcohol; for 36h; Heating;

DOI:10.1002/ardp.19843171114

upstream raw materials:

(2-chloroethyl)dimethylamine hydrochloride

((1R,2S,4R)-2-Hydroxy-1,7,7-trimethyl-bicyclo[2.2.1]hept-2-yl)-phenyl-acetic acid

((1R,2R,4R)-2-Hydroxy-1,7,7-trimethyl-bicyclo[2.2.1]hept-2-yl)-phenyl-acetic acid

((1R,2S,4R)-2-Hydroxy-1,7,7-trimethyl-bicyclo[2.2.1]hept-2-yl)-phenyl-acetic acid

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