3-Butenoic acid, 4-phenoxy-, phenyl ester, (Z)-

Base Information

• Chemical Name: 3-Butenoic acid, 4-phenoxy-, phenyl ester, (Z)-
• CAS No.: 114524-39-9
• Molecular Formula: C₁₆H₁₄O₃
• Molecular Weight: 254.285
• Mol file: 114524-39-9.mol

Synonyms:

Chemical Property of 3-Butenoic acid, 4-phenoxy-, phenyl ester, (Z)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-Butenoic acid, 4-phenoxy-, phenyl ester, (Z)-

There total 3 articles about 3-Butenoic acid, 4-phenoxy-, phenyl ester, (Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl-4-bromo-2-butenoate (1117-71-1,56699-18-4,6000-00-6) + phenol (108-95-2,27073-41-2) → (Z)-4-Phenoxy-but-3-enoic acid methyl ester (114524-37-7) + (Z)-4-Phenoxy-but-3-enoic acid phenyl ester (114524-39-9)

Guidance literature:

With sodium methylate; In methanol; for 8h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;

DOI:10.1016/S0040-4020(01)90295-9

Reference yield:

methyl-4-bromo-2-butenoate (1117-71-1,56699-18-4,6000-00-6) + phenol (108-95-2,27073-41-2) → methyl γ-phenoxycrotonate (114524-36-6) + (E)-4-Phenoxy-but-2-enoic acid phenyl ester (114524-38-8) + (Z)-4-Phenoxy-but-3-enoic acid phenyl ester (114524-39-9)

Guidance literature:

With sodium hydroxide; In methanol; for 8h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;

DOI:10.1016/S0040-4020(01)90295-9

Reference yield:

methyl-4-bromo-2-butenoate (1117-71-1,56699-18-4,6000-00-6) + phenol (108-95-2,27073-41-2) → methyl γ-phenoxycrotonate (114524-36-6) + (Z)-4-Phenoxy-but-3-enoic acid methyl ester (114524-37-7) + (E)-4-Phenoxy-but-2-enoic acid phenyl ester (114524-38-8) + (Z)-4-Phenoxy-but-3-enoic acid phenyl ester (114524-39-9)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; for 8h; Product distribution; Ambient temperature; further reagents, solvents, reaction temperature, and time.;

DOI:10.1016/S0040-4020(01)90295-9

upstream raw materials:

methyl-4-bromo-2-butenoate

phenol