Stannane, (1-pentyl-1-heptenyl)triphenyl-, (E)-

Base Information

Chemical Name:Stannane, (1-pentyl-1-heptenyl)triphenyl-, (E)-
CAS No.:114566-78-8
Molecular Formula:C₃₀H₃₈Sn
Molecular Weight:517.342
Hs Code.:
Mol file:114566-78-8.mol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Stannane, (1-pentyl-1-heptenyl)triphenyl-, (E)-

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Technology Process of Stannane, (1-pentyl-1-heptenyl)triphenyl-, (E)-

There total 1 articles about Stannane, (1-pentyl-1-heptenyl)triphenyl-, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 6975-99-1
6-dodecyne

: 892-20-6
triphenylstannane

: 107711-43-3,114566-78-8
C₅H₁₁CHCC₅H₁₁Sn(C₆H₅)3

Guidance literature:: triethyl borane; In hexane; toluene; addn. of Et3B in hexane to a soln. of (n-C5H11)CC and Ph3SnH in toluene at 25°C under Ar, stirring for 10 h; pouring into water, extg. 3 times with ethyl acetate, washing the combined org. layers with brine, drying over Na2SO4, concg. in vac., preparative TLC on silica gel;
DOI:10.1021/ja00242a068