4-Methyl-1-(prop-2-en-1-yl)-1h-imidazole

Base Information

Chemical Name:4-Methyl-1-(prop-2-en-1-yl)-1h-imidazole
CAS No.:6307-15-9
Molecular Formula:C7H10N2
Molecular Weight:122.1677
Hs Code.:
NSC Number:41090
DSSTox Substance ID:DTXSID80285217
Nikkaji Number:J3.502.447F
Wikidata:Q82020511

Synonyms:1-allyl-4-methyl-1H-imidazole;6307-15-9;4-methyl-1-(prop-2-en-1-yl)-1h-imidazole;NSC41090;SCHEMBL4760870;DTXSID80285217;CCCXEUIYYWUDID-UHFFFAOYSA-N;NSC-41090

Suppliers and Price of 4-Methyl-1-(prop-2-en-1-yl)-1h-imidazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 4-Methyl-1-(prop-2-en-1-yl)-1h-imidazole

Chemical Property:

Vapor Pressure:0.0551mmHg at 25°C
Boiling Point:241.7°Cat760mmHg
Flash Point:100°C
Density:0.93g/cm³
XLogP3:1.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:122.084398327
Heavy Atom Count:9
Complexity:101

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CN(C=N1)CC=C

Technology Process of 4-Methyl-1-(prop-2-en-1-yl)-1h-imidazole

There total 3 articles about 4-Methyl-1-(prop-2-en-1-yl)-1h-imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 822-36-6
4-methyl-1H-imidazole

: 106-95-6
allyl bromide

: 6307-15-9
1-allyl-4-methylimidazole

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 822-36-6
4-methyl-1H-imidazole

: 106-95-6
allyl bromide

: 6307-15-9
1-allyl-4-methylimidazole

: 1-allyl-5-methylimidazole

Guidance literature:: 4-methyl-1H-imidazole; With sodium hydride; In tetrahydrofuran; for 1h; Reflux;

allyl bromide; In tetrahydrofuran; at 50 ℃; for 3h; Overall yield = 41 %;
DOI:10.1021/acs.orglett.6b00001

Reference yield:

: 822-36-6
4-methyl-1H-imidazole

: 107-18-6
allyl alcohol

: 6307-15-9
1-allyl-4-methylimidazole

: 1-allyl-5-methylimidazole

Guidance literature:: With 2,3,4,5,6-pentafluorophenol; briphos; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In dichloromethane; at 30 ℃; for 24h; Temperature; Overall yield = 96 %; Inert atmosphere;
DOI:10.1021/acs.orglett.6b00001