Benzenepentanoic acid, 2-iodo-b-oxo-, ethyl ester

Base Information

Chemical Name:Benzenepentanoic acid, 2-iodo-b-oxo-, ethyl ester
CAS No.:114657-40-8
Molecular Formula:C₁₃H₁₅IO₃
Molecular Weight:346.165
Hs Code.:

Synonyms:

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Chemical Property of Benzenepentanoic acid, 2-iodo-b-oxo-, ethyl ester

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Technology Process of Benzenepentanoic acid, 2-iodo-b-oxo-, ethyl ester

There total 1 articles about Benzenepentanoic acid, 2-iodo-b-oxo-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 40400-13-3
2-Iodobenzyl bromide

: 141-97-9
ethyl acetoacetate

: 114657-40-8
ethyl 5-(2-iodophenyl)-3-oxopentanoate

Guidance literature:: With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; for 10h; Ambient temperature;

Reference yield:

: 114657-40-8
ethyl 5-(2-iodophenyl)-3-oxopentanoate

: 114657-47-5
1,5-bis(2-ethynylphenyl)pentan-3-one

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) anhydrous potassium carbonate; 2.) 20 percent aqueous sulphuric acid, acetic acid / 1.) acetone, reflux, 11 h; 2.) reflux, 10 h

2: 58 percent / copper(I) iodide, tetrakis(triphenylphosphine)palladium⁽⁰⁾ / triethylamine; tetrahydrofuran; hexane / 16 h / 90 °C

3: 92 percent / potassium fluoride dihydrate / dimethylformamide / 1 h / Ambient temperature

With potassium fluoride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; potassium carbonate; acetic acid; In tetrahydrofuran; hexane; triethylamine; N,N-dimethyl-formamide;

Reference yield:

: 114657-40-8
ethyl 5-(2-iodophenyl)-3-oxopentanoate

: 114657-46-4
1,5-bis(2-trimethylsilylethynylphenyl)pentan-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) anhydrous potassium carbonate; 2.) 20 percent aqueous sulphuric acid, acetic acid / 1.) acetone, reflux, 11 h; 2.) reflux, 10 h

2: 58 percent / copper(I) iodide, tetrakis(triphenylphosphine)palladium⁽⁰⁾ / triethylamine; tetrahydrofuran; hexane / 16 h / 90 °C

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; potassium carbonate; acetic acid; In tetrahydrofuran; hexane; triethylamine;