Technology Process of 2,3-Naphthalenedicarboxylic acid,
6-methoxy-1,4,5,8-tetrakis(phenylmethoxy)-
There total 6 articles about 2,3-Naphthalenedicarboxylic acid,
6-methoxy-1,4,5,8-tetrakis(phenylmethoxy)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydroxide; water;
In
tetrahydrofuran; methanol;
at 55 - 60 ℃;
for 1h;
DOI:10.1021/ja00227a030
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 98 percent / potassium carbonate / acetone / 15 h / Ambient temperature
2: 40 percent / sodium bis(trimethylsilyl)amide, 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone / tetrahydrofuran / 0.5 h
3: 82 percent / potassium carbonate / acetone / Ambient temperature
4: 6.5 g / sodium hydroxide, water / tetrahydrofuran; methanol / 1 h / 55 - 60 °C
With
1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; sodium hydroxide; water; sodium hexamethyldisilazane; potassium carbonate;
In
tetrahydrofuran; methanol; acetone;
DOI:10.1021/ja00227a030
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 98 percent / potassium carbonate / acetone / 15 h / Ambient temperature
2: 40 percent / sodium bis(trimethylsilyl)amide, 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone / tetrahydrofuran / 0.5 h
3: 82 percent / potassium carbonate / acetone / Ambient temperature
4: 6.5 g / sodium hydroxide, water / tetrahydrofuran; methanol / 1 h / 55 - 60 °C
With
1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; sodium hydroxide; water; sodium hexamethyldisilazane; potassium carbonate;
In
tetrahydrofuran; methanol; acetone;
DOI:10.1021/ja00227a030
