4-ethoxy-4'-nitrosodiphenylamine

Base Information

• Chemical Name: 4-ethoxy-4'-nitrosodiphenylamine
• CAS No.: 7696-67-5
• Molecular Formula: C₁₄H₁₄N₂O₂
• Molecular Weight: 242.277
• Mol file: 7696-67-5.mol

Synonyms:4-Ethoxy-4'-nitrosodiphenylamine;4'-Nitroso-4-aethoxy-diphenylamin;

Chemical Property of 4-ethoxy-4'-nitrosodiphenylamine

Chemical Property:

• Vapor Pressure: 1.16E-06mmHg at 25°C
• Boiling Point: 401.7°Cat760mmHg
• Flash Point: 196.7°C
• PSA: 50.69000
• Density: 1.13g/cm³
• LogP: 4.29980

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-ethoxy-4'-nitrosodiphenylamine

There total 5 articles about 4-ethoxy-4'-nitrosodiphenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-ethoxy-4-nitrosobenzene (3420-97-1) + 4-Ethoxyaniline (156-43-4) → 4'-Nitroso-4-aethoxy-diphenylamin (7696-67-5)

Guidance literature:

With hydrogenchloride;

DOI:10.1021/jo01277a039

Reference yield:

(4-ethoxy-phenyl)-nitroso-phenyl-amine → 4'-Nitroso-4-aethoxy-diphenylamin (7696-67-5)

Guidance literature:

With hydrogenchloride;

Reference yield:

4-ethoxy-N-phenylaniline (1020-54-8) → 4'-Nitroso-4-aethoxy-diphenylamin (7696-67-5)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrochloric acid; alcohol; water; sodium nitrite

2: alcoholic hydrochloric acid

With hydrogenchloride; ethanol; water; sodium nitrite;

upstream raw materials:

1-ethoxy-4-nitrosobenzene

4-Ethoxyaniline

hydrogenchloride

4-ethoxy-N-phenylaniline

Downstream raw materials:

N-(4-ethoxy-phenyl)-p-phenylenediamine

N,N'-Bis-<4-nitroso-phenyl>-p-phenylendiamin

N,N'-bis-(4-phenetidino-phenyl)-thiourea