L-Phenylalanine, N-[N-[N-[N-[(phenylmethoxy)carbonyl]glycyl]-L-phenylalanyl]-L-phenylalan yl]-, ethyl ester

Base Information

Chemical Name:L-Phenylalanine, N-[N-[N-[N-[(phenylmethoxy)carbonyl]glycyl]-L-phenylalanyl]-L-phenylalan yl]-, ethyl ester
CAS No.:116064-60-9
Molecular Formula:C₃₉H₄₂N₄O₇
Molecular Weight:678.785
Hs Code.:

Synonyms:

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Chemical Property of L-Phenylalanine, N-[N-[N-[N-[(phenylmethoxy)carbonyl]glycyl]-L-phenylalanyl]-L-phenylalan yl]-, ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of L-Phenylalanine, N-[N-[N-[N-[(phenylmethoxy)carbonyl]glycyl]-L-phenylalanyl]-L-phenylalan yl]-, ethyl ester

There total 1 articles about L-Phenylalanine, N-[N-[N-[N-[(phenylmethoxy)carbonyl]glycyl]-L-phenylalanyl]-L-phenylalan yl]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1738-86-9
Z-Gly-ONp

: 74973-88-9
Z-Phe-Phe-Phe-OEt

: 116064-60-9
(S)-2-{(S)-2-[(S)-2-(2-Benzyloxycarbonylamino-acetylamino)-3-phenyl-propionylamino]-3-phenyl-propionylamino}-3-phenyl-propionic acid ethyl ester

Guidance literature:: With hydrogen bromide; acetic acid; triethylamine; Yield given. Multistep reaction; 1.)anisol 1 h; 2.) THF, 3 day;

Reference yield:

: 116064-60-9
(S)-2-{(S)-2-[(S)-2-(2-Benzyloxycarbonylamino-acetylamino)-3-phenyl-propionylamino]-3-phenyl-propionylamino}-3-phenyl-propionic acid ethyl ester

: 116064-61-0
Boc-Arg(NO₂)-Glu(OBzl)-Gly-Phe-Phe-Phe-OEt

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 25percent HBr, AcOH; 2.) triethylamine / 1.) anisol, 1 h; 2.) DMF, 3 day

2: 2.) N-methylmorpholine, isobutylchloroformate / 2.) -11 deg C, DMF

With 4-methyl-morpholine; hydrogen bromide; acetic acid; triethylamine; isobutyl chloroformate;

Reference yield:

: 116064-60-9
(S)-2-{(S)-2-[(S)-2-(2-Benzyloxycarbonylamino-acetylamino)-3-phenyl-propionylamino]-3-phenyl-propionylamino}-3-phenyl-propionic acid ethyl ester

: Boc-Lys(Z)-Asp(OBzl)-Gly-Phe-Phe-Phe-OEt

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 25percent HBr, AcOH; 2.) triethylamine / 1.) anisol, 1 h; 2.) DMF, 3 day

With hydrogen bromide; acetic acid; triethylamine;