3H-1,2,4-Triazolo[4,3-b][1,2,4]triazole-3-thione, 7-(4-chlorophenyl)-6-[(4-chlorophenyl)amino]-2,7-dihydro-2-methyl-

Base Information

Chemical Name:3H-1,2,4-Triazolo[4,3-b][1,2,4]triazole-3-thione, 7-(4-chlorophenyl)-6-[(4-chlorophenyl)amino]-2,7-dihydro-2-methyl-
CAS No.:116088-31-4
Molecular Formula:C16H12Cl2N6S
Molecular Weight:391.283
Hs Code.:
Mol file:116088-31-4.mol

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Chemical Property of 3H-1,2,4-Triazolo[4,3-b][1,2,4]triazole-3-thione, 7-(4-chlorophenyl)-6-[(4-chlorophenyl)amino]-2,7-dihydro-2-methyl-

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Technology Process of 3H-1,2,4-Triazolo[4,3-b][1,2,4]triazole-3-thione, 7-(4-chlorophenyl)-6-[(4-chlorophenyl)amino]-2,7-dihydro-2-methyl-

There total 2 articles about 3H-1,2,4-Triazolo[4,3-b][1,2,4]triazole-3-thione, 7-(4-chlorophenyl)-6-[(4-chlorophenyl)amino]-2,7-dihydro-2-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 116088-24-5
4-(N,N'-bis(4-chlorophenyl)guanidino-2methyl-5-methylthio-2H-1,2,4-triazole-3(4H)-thione

: 116088-31-4
7-(4-chlorophenyl)-6-(4-chlorophenyl)amino-2-methyltriazolo-triazolethione

Guidance literature:: With potassium tert-butylate; In tert-butyl alcohol; for 24h; Heating;
DOI:10.1039/P19870002667

Reference yield:

: 1220-00-4
1,3-bis(4-chlorophenyl)thiourea

: 116088-31-4
7-(4-chlorophenyl)-6-(4-chlorophenyl)amino-2-methyltriazolo-triazolethione

Guidance literature:: Multi-step reaction with 2 steps

1: 41 percent / toluene / 24 h / Heating

2: 90 percent / potassium t-butoxide / 2-methyl-propan-2-ol / 24 h / Heating

With potassium tert-butylate; In toluene; tert-butyl alcohol;
DOI:10.1039/P19870002667