1-Butanol, 4-(triphenylstannyl)-

Base Information

Chemical Name:1-Butanol, 4-(triphenylstannyl)-
CAS No.:116195-74-5
Molecular Formula:C22H24OSn
Molecular Weight:423.142
Hs Code.:
Mol file:116195-74-5.mol

Synonyms:

Suppliers and Price of 1-Butanol, 4-(triphenylstannyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1-Butanol, 4-(triphenylstannyl)-

Chemical Property:

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-Butanol, 4-(triphenylstannyl)-

There total 6 articles about 1-Butanol, 4-(triphenylstannyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 114599-29-0
(C₆H₅)3Sn(CH₂)3COOCH₃

: 116195-74-5
4-triphenylstannyl-butan-1-ol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; heated at reflux;;

Reference yield:

: 639-58-7
triphenyltin chloride

: 116195-74-5
4-triphenylstannyl-butan-1-ol

Guidance literature:: With tetrahydrofuran; 1,2,3-trimethylallylbromide; magnesium; In tetrahydrofuran; THF added to Mg and react. initiated by addn. 1,1,2-trimethylallylbromide; soln. heated to reflux and soln. of Ph3SnCl in THF and 1,1,2-trimethylallylbromide added over 2.5 h; mixt. stirred for 22 h; hydrolyzed withNH4Cl soln.; organic layer isolated, solvent removed by evapn., bis-allyls distilledoff (68-70°C at 12 torr), residue dissolved in ether, washed with MeOH-water soln. KF, ether layer dried with MgSO4, ether removed, product crystd. from hexane; elem. anal.;
DOI:10.1016/S0020-1693(00)87781-6