4-methyl-2-propylaniline

Base Information

• Chemical Name: 4-methyl-2-propylaniline
• CAS No.: 116436-12-5
• Molecular Formula: C10H15N
• Molecular Weight: 149.236
• Mol file: 116436-12-5.mol

Synonyms:

Chemical Property of 4-methyl-2-propylaniline

Chemical Property:

• Vapor Pressure: 0.0254mmHg at 25°C

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-methyl-2-propylaniline

There total 8 articles about 4-methyl-2-propylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

2-allyl-4-methyl-phenylamine (59816-83-0) → 4-methyl-2-propyl-aniline (116436-12-5)

Guidance literature:

With iron(II)β-diketiminate complex; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; In benzene-d6; at 20 ℃; for 0.5h; Sealed tube; Inert atmosphere; Schlenk technique; Glovebox;

DOI:10.1021/jacs.8b11553

Reference yield:

C17H20N2O2S (32853-54-6) → 4-methyl-2-propyl-aniline (116436-12-5)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol;

DOI:10.1002/hlca.19710540402

Reference yield:

4-Allyl-4-methyl-cyclohexa-2,5-dien-1-on-p-toluolsulfonyl-hydrazon (32853-52-4) → 4-methyl-2-propyl-aniline (116436-12-5)

Guidance literature:

Multi-step reaction with 2 steps

1: aq. HCl / methanol

2: H₂ / Pd-C / methanol

With hydrogenchloride; hydrogen; palladium on activated charcoal; In methanol;

DOI:10.1002/hlca.19710540402

upstream raw materials:

2,5-Dimethyl-1H-indole

C₁₇H₂₀N₂O₂S

decalin

4-Allyl-4-methyl-cyclohexa-2,5-dien-1-on-p-toluolsulfonyl-hydrazon

Downstream raw materials:

2-propyl-4-methylphenol

Refernces