Benzenamine, 3-methyl-, hydrobromide

Base Information

• Chemical Name: Benzenamine, 3-methyl-, hydrobromide
• CAS No.: 116468-99-6
• Molecular Formula: Br*C₇H₁₀N
• Molecular Weight: 188.067
• Mol file: 116468-99-6.mol

Synonyms:

Chemical Property of Benzenamine, 3-methyl-, hydrobromide

Chemical Property:

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenamine, 3-methyl-, hydrobromide

There total 1 articles about Benzenamine, 3-methyl-, hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-ethyl-2-bromo-pyridinium; bromide (79343-93-4) + 1-amino-3-methylbenzene (108-44-1) → meta-toluidinium bromide (116468-99-6) + 1-Ethyl-2-m-tolylamino-pyridinium; bromide

Guidance literature:

In acetonitrile; at 25 ℃; Rate constant;

Reference yield: 53.0%

methyl-m-tolyl-carbamonitrile (59709-69-2) + meta-toluidinium bromide (116468-99-6) → N-Methyl-N,N'-di-m-tolyl-guanidine; hydrobromide

Guidance literature:

at 160 ℃;

DOI:10.1021/jm00028a009

Reference yield:

sodium hexabromo osmate(IV) + meta-toluidinium bromide (116468-99-6) → m-toluidinium osmium(IV) bromide

Guidance literature:

In hydrogen bromide; bromide dissolved in dild. HBr added to the soln. of Na2{OsBr6} at common temp.; excess of Os-soln.; crystalline or oily product;; crystn. of the oily product by grinding or by dissoln. in hot alcohol and cooling or evapn. of the soln.; crystn. by addn. of small amounts of HBr (with some drops of alc.) to the product in mother liquor at higher temp.;;

upstream raw materials:

1-ethyl-2-bromo-pyridinium; bromide

1-amino-3-methylbenzene