Acetic acid, chloro((2-chlorophenyl)hydrazono)-, methyl ester

Base Information

Chemical Name:Acetic acid, chloro((2-chlorophenyl)hydrazono)-, methyl ester
CAS No.:82417-83-2
Molecular Formula:C9H8Cl2N2O2
Molecular Weight:247.078
Hs Code.:

Synonyms:82417-83-2;Acetic acid, chloro((2-chlorophenyl)hydrazono)-, methyl ester;methyl (2Z)-2-chloro-2-[(2-chlorophenyl)hydrazinylidene]acetate;Methyl chloro[(2-chlorophenyl)hydrazono]acetate;Methyl (2Z)-chloro[2-(2-chlorophenyl)hydrazinylidene]ethanoate;MFCD03175037;AKOS037629353

Suppliers and Price of Acetic acid, chloro((2-chlorophenyl)hydrazono)-, methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Acetic acid, chloro((2-chlorophenyl)hydrazono)-, methyl ester

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:318°Cat760mmHg
Flash Point:146.1°C
Density:1.37g/cm³
XLogP3:5.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:245.9962829
Heavy Atom Count:15
Complexity:259

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC(=O)C(=NNC1=CC=CC=C1Cl)Cl
Isomeric SMILES:COC(=O)/C(=N/NC1=CC=CC=C1Cl)/Cl

Technology Process of Acetic acid, chloro((2-chlorophenyl)hydrazono)-, methyl ester

There total 1 articles about Acetic acid, chloro((2-chlorophenyl)hydrazono)-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4755-81-1,935731-92-3
methyl 2-chloroacetoacetate

: 95-51-2
o-chloroaniline

: 82417-83-2
chloro[(2-chlorophenyl)hydrazono]-acetic acid, methyl ester

Guidance literature:: With hydrogenchloride; sodium acetate; sodium nitrite; Multistep reaction; 1.) water; 2.) ethanol-water, 0 deg C, 3 h, overnight;

Reference yield: 87.0%

: 5281-18-5
benzaldehyde, hydrazone

: 82417-83-2
chloro[(2-chlorophenyl)hydrazono]-acetic acid, methyl ester

: 82418-43-7
Methyl-2-benzylidenhydrazino-2-(2-chlorphenylhydrazono)acetat

Guidance literature:: With triethylamine; In acetonitrile; at 50 ℃; for 2h;

Reference yield:

: 82417-83-2
chloro[(2-chlorophenyl)hydrazono]-acetic acid, methyl ester

: 96723-20-5
1-(2-Chloro-phenyl)-5-phenyl-1H-pyrazole-3,4-dicarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium ethoxide; 3.) dry HCl / 1.) ethanol, 20 min; 2.) ethanol, RT, 48 h,; 3.) reflux, 3 h

2: 79 percent / 10percent aq. sodium hydroxide / ethanol / 2 h / Heating

With hydrogenchloride; sodium hydroxide; sodium ethanolate; In ethanol;