3-Buten-1-ol, 4-(triphenylgermyl)-, (Z)-

Base Information

Chemical Name:3-Buten-1-ol, 4-(triphenylgermyl)-, (Z)-
CAS No.:116524-24-4
Molecular Formula:C22H22GeO
Molecular Weight:375.006
Hs Code.:
Mol file:116524-24-4.mol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Buten-1-ol, 4-(triphenylgermyl)-, (Z)-

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Technology Process of 3-Buten-1-ol, 4-(triphenylgermyl)-, (Z)-

There total 2 articles about 3-Buten-1-ol, 4-(triphenylgermyl)-, (Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 2816-43-5
triphenylgermane

: 927-74-2
3-Butyn-1-ol

: 116524-24-4
(Z)-4-triphenylgermyl-3-buten-1-ol

Guidance literature:: triethyl borane; In hexane; toluene; addn. of Et3B in hexane to a soln. of acetylene-compd. and Ph3GeH in toluene under Ar, stirring for 5 h at -78°C; purifn. by column chromy. or preparative thin-layer chromy. on silica gel,; elem. anal.; isomer ratio Z/E=>20/1 (detd. by GC, NMR);
DOI:10.1246/bcsj.63.2268