1,4-Dioxin, 2,3-dihydro-5-(2,6,6-trimethyl-1-cyclohexen-1-yl)-

Base Information

Chemical Name:1,4-Dioxin, 2,3-dihydro-5-(2,6,6-trimethyl-1-cyclohexen-1-yl)-
CAS No.:116809-86-0
Molecular Formula:C13H20O2
Molecular Weight:208.301
Hs Code.:
DSSTox Substance ID:DTXSID60449259
Wikidata:Q82268672
Mol file:116809-86-0.mol

Synonyms:116809-86-0;1,4-Dioxin, 2,3-dihydro-5-(2,6,6-trimethyl-1-cyclohexen-1-yl)-;DTXSID60449259

Suppliers and Price of 1,4-Dioxin, 2,3-dihydro-5-(2,6,6-trimethyl-1-cyclohexen-1-yl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1,4-Dioxin, 2,3-dihydro-5-(2,6,6-trimethyl-1-cyclohexen-1-yl)-

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:208.146329876
Heavy Atom Count:15
Complexity:311

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(CCC1)(C)C)C2=COCCO2

Technology Process of 1,4-Dioxin, 2,3-dihydro-5-(2,6,6-trimethyl-1-cyclohexen-1-yl)-

There total 2 articles about 1,4-Dioxin, 2,3-dihydro-5-(2,6,6-trimethyl-1-cyclohexen-1-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 116809-79-1,116809-80-4
2,2,6-trimethyl-1-<2-(1,4-dioxenyl)>-1-cyclohexanol

: 116809-86-0
2,6,6-trimethyl-1-<2-(1,4-dioxenyl)>-1-cyclohexene

Guidance literature:: With 4 A molecular sieve; In benzene; for 72h; Ambient temperature;
DOI:10.1021/jo00259a012

Reference yield:

: 2408-37-9
2,2,6-trimethylcyclohexan-1-one

: 116809-86-0
2,6,6-trimethyl-1-<2-(1,4-dioxenyl)>-1-cyclohexene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) t-BuLi / 1.) pentane, -20 deg C, 2 h, 2.) THF, -10 deg C, 2 h

2: 93 percent / molecular sieves 4A / benzene / 72 h / Ambient temperature

With 4 A molecular sieve; tert.-butyl lithium; In benzene;
DOI:10.1021/jo00259a012