Benzenamine, 3-[(2-propen-1-yloxy)methyl]-

Base Information

Chemical Name:Benzenamine, 3-[(2-propen-1-yloxy)methyl]-
CAS No.:117401-78-2
Molecular Formula:C10H13NO
Molecular Weight:163.219
Hs Code.:
DSSTox Substance ID:DTXSID301278312
Mol file:117401-78-2.mol

Synonyms:117401-78-2;3-allyloxymethyl-phenylamine;Benzenamine, 3-[(2-propen-1-yloxy)methyl]-;3-(prop-2-enoxymethyl)aniline;3-[(prop-2-en-1-yloxy)methyl]aniline;3-((Allyloxy)methyl)aniline;SCHEMBL823910;DTXSID301278312;3-[(2-Propen-1-yloxy)methyl]benzenamine;A1-29239

Suppliers and Price of Benzenamine, 3-[(2-propen-1-yloxy)methyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of Benzenamine, 3-[(2-propen-1-yloxy)methyl]-

Chemical Property:

XLogP3:1.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:163.099714038
Heavy Atom Count:12
Complexity:136

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C=CCOCC1=CC(=CC=C1)N

Technology Process of Benzenamine, 3-[(2-propen-1-yloxy)methyl]-

There total 2 articles about Benzenamine, 3-[(2-propen-1-yloxy)methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 117401-73-7
1-allyloxymethyl-3-nitrobenzene

: 117401-78-2
3-allyloxymethylphenylamine

Guidance literature:: With tin(ll) chloride; In ethanol; at 70 ℃; for 0.5h;
DOI:10.1016/S0040-4020(01)81575-1

Reference yield:

: 619-25-0
3-Nitrobenzyl alcohol

: 117401-78-2
3-allyloxymethylphenylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 1) KOtBu / 1) THF, 0 deg C, 10 min, 2a) 0 deg C, 80 min, b) up to r. t., 1 h, c) 50 deg C, 6 h

2: 94 percent / SnCl₂*2H₂O / aq. ethanol / 0.5 h / 70 °C

With potassium tert-butylate; tin(ll) chloride; In ethanol;
DOI:10.1016/S0040-4020(01)81575-1