[4-(5-allyloxymethylfuran-2-yl)pyrimidin-2-yl]-(3-allyloxymethylphenyl)amine

Base Information

Chemical Name:[4-(5-allyloxymethylfuran-2-yl)pyrimidin-2-yl]-(3-allyloxymethylphenyl)amine
CAS No.:1364123-93-2
Molecular Formula:C₂₂H₂₃N₃O₃
Molecular Weight:377.443
Hs Code.:

Synonyms:[4-(5-allyloxymethylfuran-2-yl)pyrimidin-2-yl]-(3-allyloxymethylphenyl)amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [4-(5-allyloxymethylfuran-2-yl)pyrimidin-2-yl]-(3-allyloxymethylphenyl)amine

Chemical Property:

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Technology Process of [4-(5-allyloxymethylfuran-2-yl)pyrimidin-2-yl]-(3-allyloxymethylphenyl)amine

There total 6 articles about [4-(5-allyloxymethylfuran-2-yl)pyrimidin-2-yl]-(3-allyloxymethylphenyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 937271-54-0
4-(5-allyloxymethylfuran-2-yl)-2-chloropyrimidine

: 117401-78-2
3-allyloxymethylphenylamine

: 1364123-93-2
[4-(5-allyloxymethylfuran-2-yl)pyrimidin-2-yl]-(3-allyloxymethylphenyl)amine

Guidance literature:: With hydrogenchloride; water; In butan-1-ol; at 80 - 100 ℃; for 12h;
DOI:10.1021/jm201454n

Reference yield:

: 619-25-0
3-Nitrobenzyl alcohol

: 1364123-93-2
[4-(5-allyloxymethylfuran-2-yl)pyrimidin-2-yl]-(3-allyloxymethylphenyl)amine

Guidance literature:: Multi-step reaction with 3 steps

1: tetra(n-butyl)ammonium hydrogensulfate; potassium hydroxide / 12 h / 20 °C

2: tin(II) chloride dihdyrate / methanol; dichloromethane / 0 - 20 °C

3: hydrogenchloride; water / butan-1-ol / 12 h / 80 - 100 °C

With hydrogenchloride; tin(II) chloride dihdyrate; water; tetra(n-butyl)ammonium hydrogensulfate; potassium hydroxide; In methanol; dichloromethane; butan-1-ol;
DOI:10.1021/jm201454n

Reference yield:

: 937271-52-8
5-(2-chloropyrimidin-4-yl)furan-2-carbaldehyde

: 1364123-93-2
[4-(5-allyloxymethylfuran-2-yl)pyrimidin-2-yl]-(3-allyloxymethylphenyl)amine

Guidance literature:: Multi-step reaction with 3 steps

1: methanol; sodium tetrahydroborate / tetrahydrofuran / 0 - 20 °C

2: tetra(n-butyl)ammonium hydrogensulfate; potassium hydroxide / 12 h / 20 °C

3: hydrogenchloride; water / butan-1-ol / 12 h / 80 - 100 °C

With hydrogenchloride; methanol; sodium tetrahydroborate; water; tetra(n-butyl)ammonium hydrogensulfate; potassium hydroxide; In tetrahydrofuran; butan-1-ol;
DOI:10.1021/jm201454n