4-[2-(2-Ethoxyethoxy)ethoxy]benzaldehyde

Base Information

• Chemical Name: 4-[2-(2-Ethoxyethoxy)ethoxy]benzaldehyde
• CAS No.: 117420-31-2
• Molecular Formula: C13H18O4
• Molecular Weight: 238.284
• DSSTox Substance ID: DTXSID90392961
• Wikidata: Q82191512
• Mol file: 117420-31-2.mol

Synonyms:4-[2-(2-ethoxyethoxy)ethoxy]benzaldehyde;117420-31-2;SCHEMBL9484385;DTXSID90392961

Chemical Property of 4-[2-(2-Ethoxyethoxy)ethoxy]benzaldehyde

Chemical Property:

• XLogP3: 1.4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 9
• Exact Mass: 238.12050905
• Heavy Atom Count: 17
• Complexity: 188

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CCOCCOCCOC1=CC=C(C=C1)C=O

Technology Process of 4-[2-(2-Ethoxyethoxy)ethoxy]benzaldehyde

There total 3 articles about 4-[2-(2-Ethoxyethoxy)ethoxy]benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1-bromo-2-(2-ethoxyethoxy)ethane (54550-36-6) + 4-hydroxy-benzaldehyde (123-08-0,65581-83-1) → 4-(2-(2-ethoxyethoxy)ethoxy)benzaldehyde (117420-31-2)

Guidance literature:

With potassium carbonate; potassium iodide; In acetone; for 24h; Reflux;

DOI:10.1039/c4tc00720d

Reference yield:

ethoxyethoxyethanol (111-90-0) → 4-(2-(2-ethoxyethoxy)ethoxy)benzaldehyde (117420-31-2)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N / 6 h / cooling

2: K₂CO₃ / acetone / 48 h / Heating

With potassium carbonate; triethylamine; In acetone;

DOI:10.1016/j.jorganchem.2004.11.010

Reference yield:

1-ethoxy-2-(2-(2-iodoethoxy)ethoxy)ethane (126750-26-3) + 4-hydroxy-benzaldehyde (123-08-0,65581-83-1) → 4-(2-(2-ethoxyethoxy)ethoxy)benzaldehyde (117420-31-2)

Guidance literature:

With sodium hydroxide; Yield given. Multistep reaction; 1.) butyl alcolhol, reflux, 1 h, 2.) reflux, 12 h;

upstream raw materials:

1-ethoxy-2-(2-(2-iodoethoxy)ethoxy)ethane

4-hydroxy-benzaldehyde

ethoxyethoxyethanol

1-bromo-2-(2-ethoxyethoxy)ethane

Downstream raw materials:

C₂₅H₃₁BF₂N₂O₃

3-<(p-ethoxyethoxyethoxyphenyl)(4-phenyl-3,5-dioxacyclohexyl)methyl>-1,5,8,11-tetraoxacyclotridecane

3,3'-(p-ethoxyethoxyethoxybenzylidene)bis(1,5,8,11-tetraoxacyclotridecane)

2-(p-ethoxyethoxyethoxyphenyl)-1,1,3,3-tetraethoxycarbonylpropane

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