Benzenemethanol, 2,5-dimethoxy-3,4,6-trimethyl-

Base Information

• Chemical Name: Benzenemethanol, 2,5-dimethoxy-3,4,6-trimethyl-
• CAS No.: 117574-74-0
• Molecular Formula: C12H18O3
• Molecular Weight: 210.273
• Mol file: 117574-74-0.mol

Synonyms:

Chemical Property of Benzenemethanol, 2,5-dimethoxy-3,4,6-trimethyl-

Chemical Property:

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzenemethanol, 2,5-dimethoxy-3,4,6-trimethyl-

There total 13 articles about Benzenemethanol, 2,5-dimethoxy-3,4,6-trimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

2,5-dimethoxy-3,4,6-trimethylbenzaldehyde (103808-42-0) → (2,5-dimethoxy-3,4,6-trimethylphenyl)methanol (117574-74-0)

Guidance literature:

With sodium tetrahydroborate; In methanol; Ambient temperature;

DOI:10.1016/S0040-4039(00)79881-9

Reference yield: 94.0%

2,5-dimethoxy-3,4,6-trimethylbenzoic acid (89048-20-4) → (2,5-dimethoxy-3,4,6-trimethylphenyl)methanol (117574-74-0)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; Heating;

Reference yield: 91.8%

1-chloromethyl-2,5-dimethoxy-3,4,6-trimethyl-benzene (54757-17-4) → (2,5-dimethoxy-3,4,6-trimethylphenyl)methanol (117574-74-0)

Guidance literature:

With water; sodium carbonate; for 48h; Heating;

DOI:10.1007/BF00473932

upstream raw materials:

1-acetoxymethyl-2,5-dimethoxy-3,4,6-trimethyl-benzene

2,5-dimethoxy-3,4,6-trimethylbenzaldehyde

1-chloromethyl-2,5-dimethoxy-3,4,6-trimethyl-benzene

2,5-dimethoxy-3,4,6-trimethylbenzoic acid

Downstream raw materials:

2-hydroxy-5-methoxy-3,4,6-trimethylbenzaldehyde

2,5-dihydroxy-3,4,6-trimethyl-benzaldehyde

2,3,5-Trimethyl-6-(2-methyl-2-nitro-propyl)-[1,4]benzoquinone

2,3,5-Trimethyl-6-nitrosooxymethyl-[1,4]benzoquinone

Refernces

• 1、 Giraud, Anne,Vanelle, Patrice,Giraud, Luc. "Radical reactions leading to substituted coumarins". . p. 4321 - 4322. Retrieved 2007/10/03.
• 2、 Riering, Helmut,Schaefer, Hans J.. "Electroorganic Synthesis, 58. Synthesis of Substituted Benzoquinones and their Use for Mediated Electrochemical Conversions". . p. 859 - 874. Retrieved 2007/10/02.