3,4-dimethyl-2-phenyl-1H-pyrrole

Base Information

Chemical Name:3,4-dimethyl-2-phenyl-1H-pyrrole
CAS No.:118799-13-6
Molecular Formula:C12H13N
Molecular Weight:171.242
Hs Code.:
DSSTox Substance ID:DTXSID50570667
Wikidata:Q82458192
Mol file:118799-13-6.mol

Synonyms:3,4-dimethyl-2-phenyl-1H-pyrrole;118799-13-6;SCHEMBL13922078;DTXSID50570667;3,4-dimethyl-2-phenyl-1H-pyrrol;AKOS006372983

Suppliers and Price of 3,4-dimethyl-2-phenyl-1H-pyrrole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 3,4-dimethyl-2-phenyl-1H-pyrrole

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:1
Exact Mass:171.104799419
Heavy Atom Count:13
Complexity:161

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CNC(=C1C)C2=CC=CC=C2

Technology Process of 3,4-dimethyl-2-phenyl-1H-pyrrole

There total 4 articles about 3,4-dimethyl-2-phenyl-1H-pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 172907-58-3
1-(Dimethylamino)-3,4-dimethyl-2-phenyl-1H-pyrrole

: 118799-13-6
3,4-Dimethyl-2-phenyl-1H-pyrrole

Guidance literature:: With ammonia; sodium; In tetrahydrofuran; for 3h; under 6000.5 - 7500.6 Torr; Ambient temperature;
DOI:10.1016/0040-4039(95)01717-V

Reference yield: 73.0%

: C₁₂H₁₃N₃

: C₁₂H₁₃NO

: 118799-13-6
3,4-Dimethyl-2-phenyl-1H-pyrrole

Guidance literature:: With silver hexafluoroantimonate; 1,1'-sulfinylbisbenzene; IPrAuCl; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1021/ja071231+

Reference yield:

: 71268-59-2
(E)-1-phenyl-1-(trimethylsiloxy)propene

: 118799-13-6
3,4-Dimethyl-2-phenyl-1H-pyrrole

Guidance literature:: Multi-step reaction with 3 steps

1: TiCl₄ / CH₂Cl₂ / 1.) -78 deg C, 15 min, 2.) -78 to -20 deg C, 3 h

2: 88 percent / p-TsOH / toluene / 4 h / Heating

3: 82 percent / Na, liq. NH₃ / tetrahydrofuran / 3 h / 6000.5 - 7500.6 Torr / Ambient temperature

With ammonia; sodium; titanium tetrachloride; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1002/jlac.199619961011