(Bromomethyl)(oxo)diphenyl-lambda~5~-phosphane

Base Information

Chemical Name:(Bromomethyl)(oxo)diphenyl-lambda~5~-phosphane
CAS No.:119460-28-5
Molecular Formula:C13H12BrOP
Molecular Weight:295.115
Hs Code.:
DSSTox Substance ID:DTXSID40554097
Wikidata:Q82434928
Mol file:119460-28-5.mol

Synonyms:119460-28-5;(Bromomethyl)(oxo)diphenyl-lambda~5~-phosphane;SCHEMBL9062983;DTXSID40554097;(Bromomethyl)diphenylphosphine oxide;bromomethyl(diphenyl)phosphine oxide

Suppliers and Price of (Bromomethyl)(oxo)diphenyl-lambda~5~-phosphane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Bromomethyl)(oxo)diphenyl-lambda~5~-phosphane

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:293.98091
Heavy Atom Count:16
Complexity:233

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)P(=O)(CBr)C2=CC=CC=C2

Technology Process of (Bromomethyl)(oxo)diphenyl-lambda~5~-phosphane

There total 4 articles about (Bromomethyl)(oxo)diphenyl-lambda~5~-phosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 884-74-2
(diphenylphosphinoyl)methanol

: 119460-28-5
bromomethyl(diphenyl)phosphine oxide

Guidance literature:: With phosphorus tribromide; In benzene; Reflux;
DOI:10.1134/S1070363212100052

Reference yield: 74.0%

: 33730-69-7
(diphenylphosphoryl)methyl p-toluenesulfonate

: 119460-28-5
bromomethyl(diphenyl)phosphine oxide

Guidance literature:: With potassium bromide; In N,N-dimethyl-formamide; for 3h; Heating;

Reference yield:

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 119460-28-5
bromomethyl(diphenyl)phosphine oxide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / water / 16 h / 100 °C

2: phosphorus tribromide / benzene / 5 h / Molecular sieve; Reflux

With hydrogenchloride; phosphorus tribromide; In water; benzene;
DOI:10.1039/c9ob02700a