Borate(1-), tetrakis(3,5-difluorophenyl)-, sodiuM(1:1)

Base Information

• Chemical Name: Borate(1-), tetrakis(3,5-difluorophenyl)-, sodiuM(1:1)
• CAS No.: 119861-51-7
• Molecular Formula: C24H12BF8.Na
• Molecular Weight: 486.147
• Mol file: 119861-51-7.mol

Synonyms:tetrakis(3,5-difluorophenyl)borate sodium salt;

Chemical Property of Borate(1-), tetrakis(3,5-difluorophenyl)-, sodiuM(1:1)

Chemical Property:

• PSA: 0.00000
• LogP: 4.17680

Purity/Quality:

97-99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Borate(1-), tetrakis(3,5-difluorophenyl)-, sodiuM(1:1)

There total 3 articles about Borate(1-), tetrakis(3,5-difluorophenyl)-, sodiuM(1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

sodium tetrafluoroborate (13755-29-8) + 3,5-difluorobromobenzene (461-96-1) → NaBARF (119861-51-7)

Guidance literature:

With magnesium; In tetrahydrofuran; diethyl ether; for 1h; Inert atmosphere; Reflux;

DOI:10.1021/acs.organomet.8b00215

Reference yield:

3,5-difluorobromobenzene (461-96-1) + boron trifluoride diethyl etherate (109-63-7) → NaBARF (119861-51-7)

Guidance literature:

3,5-difluorobromobenzene; With magnesium; In diethyl ether; at 0 ℃; for 4h;

boron trifluoride diethyl etherate; In diethyl ether; at 20 ℃; for 17h;

With sodium carbonate; In diethyl ether; water; at 20 ℃; for 24.5h;

Reference yield:

3,5-difluorobromobenzene (461-96-1) → NaBARF (119861-51-7)

Guidance literature:

With sodium carbonate; In diethyl ether; water;

upstream raw materials:

3,5-difluorobromobenzene

boron trifluoride diethyl etherate

sodium tetrafluoroborate