Acetic acid, (benzoylamino)(diethoxyphosphinyl)-, methyl ester

Base Information

Chemical Name:Acetic acid, (benzoylamino)(diethoxyphosphinyl)-, methyl ester
CAS No.:120367-99-9
Molecular Formula:C14H20NO6P
Molecular Weight:329.29
Hs Code.:
DSSTox Substance ID:DTXSID00473290
Mol file:120367-99-9.mol

Synonyms:120367-99-9;Acetic acid, (benzoylamino)(diethoxyphosphinyl)-, methyl ester;DTXSID00473290

Suppliers and Price of Acetic acid, (benzoylamino)(diethoxyphosphinyl)-, methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetic acid, (benzoylamino)(diethoxyphosphinyl)-, methyl ester

Chemical Property:

XLogP3:1.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:9
Exact Mass:329.10282436
Heavy Atom Count:22
Complexity:412

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOP(=O)(C(C(=O)OC)NC(=O)C1=CC=CC=C1)OCC

Technology Process of Acetic acid, (benzoylamino)(diethoxyphosphinyl)-, methyl ester

There total 5 articles about Acetic acid, (benzoylamino)(diethoxyphosphinyl)-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 21286-78-2,56538-58-0
methyl N-benzoyl-2-methoxyglycinate

: 122-52-1
triethyl phosphite

: 120367-99-9
methyl 2-benzamido-2-(diethoxyphosphoryl)-acetate

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -10 - 25 ℃;
DOI:10.1016/S0040-4039(00)80523-7

Reference yield:

: 19791-95-8,19791-97-0,16555-77-4
α-hydroxyhippuric acid

: 120367-99-9
methyl 2-benzamido-2-(diethoxyphosphoryl)-acetate

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid

2: 72 percent / BF₃*OEt₂ / CH₂Cl₂ / -10 - 25 °C

With sulfuric acid; boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1016/S0040-4039(00)80523-7

Reference yield:

: 114684-69-4
methyl 2-(benzyloxycarbonylamino)-2-(diethyloxyphosphoryl)acetate

: 120367-99-9
methyl 2-benzamido-2-(diethoxyphosphoryl)-acetate

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / methanol / Inert atmosphere

2: pyridine / -5 - 9 °C / Inert atmosphere

With pyridine; palladium 10% on activated carbon; hydrogen; In methanol;