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Indium, dichloro(2,4,6-trimethylphenyl)-

Base Information
  • Chemical Name:Indium, dichloro(2,4,6-trimethylphenyl)-
  • CAS No.:121866-61-3
  • Molecular Formula:C9H11Cl2In
  • Molecular Weight:304.912
  • Hs Code.:
Indium, dichloro(2,4,6-trimethylphenyl)-

Synonyms:

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Chemical Property of Indium, dichloro(2,4,6-trimethylphenyl)-
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Technology Process of Indium, dichloro(2,4,6-trimethylphenyl)-

There total 1 articles about Indium, dichloro(2,4,6-trimethylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In benzene; under N2, refluxing a mixture of INCl3 (2 equiv) and INMes3 in benzene, 12 h,; filtration, washing with C6H6 (2x) and pentane, elem. anal.;
DOI:10.1021/om00111a018
Guidance literature:
In diethyl ether; byproducts: LiCl; suspn. of As compd. in Et2O added to suspn. of In compds. in Et2O at -78°C dropwise, stirred at 20°C for 18 h; solvent evapd. in vac., residue dissolved in toluene, filtered, concd. in vac., crystd. at 5°C for several d, elem. anal.;
DOI:10.1002/zaac.200300022
Guidance literature:
In diethyl ether; Ar-atmosphere; stirring (-78°C to room temp., 3 h, room temp., 18h); evapn. (vac.), toluene addn., filtering, evapn. (vac.), n-pentane addn.,filtering, washing (n-pentane, Et2O), recrystn. (n-pentane / THF); elem . anal.;
DOI:10.1021/om960077p
upstream raw materials:

trimesitylindium

indium(III) chloride

Downstream raw materials:

{(CH3)3C6H2(Cl)InN(Si(CH3)3)2}

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