1-Aza-2-sila-5-boracyclopent-3-ene, 4,5-diethyl-2,3-dimethyl-2-phenyl-

Base Information

Chemical Name:1-Aza-2-sila-5-boracyclopent-3-ene, 4,5-diethyl-2,3-dimethyl-2-phenyl-
CAS No.:122293-31-6
Molecular Formula:C₁₄H₂₂BNSi
Molecular Weight:243.232
Hs Code.:

Synonyms:

Suppliers and Price of 1-Aza-2-sila-5-boracyclopent-3-ene, 4,5-diethyl-2,3-dimethyl-2-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of 1-Aza-2-sila-5-boracyclopent-3-ene, 4,5-diethyl-2,3-dimethyl-2-phenyl-

Chemical Property:

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-Aza-2-sila-5-boracyclopent-3-ene, 4,5-diethyl-2,3-dimethyl-2-phenyl-

There total 1 articles about 1-Aza-2-sila-5-boracyclopent-3-ene, 4,5-diethyl-2,3-dimethyl-2-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 125824-78-4
4,5,5-triethyl-2,5-dihydro-2,3-dimethyl-2-phenyl-1H-1,2,5-azoniasilaboratole

: 122293-31-6
NHSi(CH₃)(C₆H₅)C(CH₃)C(C₂H₅)B(C₂H₅)

Guidance literature:: In neat (no solvent); byproducts: C2H6; heating of the NH-1,2,5-azoniasilaboratole at 170-210°C for 3 h; distn.; elem. anal.;

Reference yield: 91.0%

: 15321-51-4
diiron nonacarbonyl

: 122293-31-6
NHSi(CH₃)(C₆H₅)C(CH₃)C(C₂H₅)B(C₂H₅)

: 122293-41-8
tricarbonyl(η4-4,5-diethyl-2,5-dihydro-2,3-dimethyl-exo-2-phenyl-1H-1,2,5-azasilaborole)iron

Guidance literature:: In 1,2,5-trimethyl-benzene; byproducts: CO; (Ar); azasilaborole and Fe complex were heated in mesitylene for 10 h at 150°C; filtered mixt. was concd. at 0,001 Torr, residue was crystd. from pentane at -80°C; elem. anal.;

Reference yield: 56.0%

: 13463-40-6,37220-42-1
iron pentacarbonyl

: 122293-31-6
NHSi(CH₃)(C₆H₅)C(CH₃)C(C₂H₅)B(C₂H₅)

: 122293-41-8,142037-87-4,122332-03-0
tricarbonyl(η4-4,5-diethyl-2,5-dihydro-2,3-dimethyl-exo/endo-2-phenyl-1H-1,2,5-azasilaborole)iron

Guidance literature:: In tetrahydrofuran; byproducts: CO; Irradiation (UV/VIS); (Ar); soln. of azasilaborole and Fe complex was irradiated for 4 h at room temp.; THF was removed in vac., residue crystd. from pentane at -78°C, concd. mother liquor yielded further fraction; mixt. of exo/endo isomers 9,5/90,5%;