Technology Process of 4,5,5-triethyl-2,5-dihydro-2,3-dimethyl-2-phenyl-1H-1,2,5-azoniasilaboratole
There total 1 articles about 4,5,5-triethyl-2,5-dihydro-2,3-dimethyl-2-phenyl-1H-1,2,5-azoniasilaboratole which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
diethyl ether;
byproducts: KCl; to the K-1,2,5-azasilaboratole in Et2O is dropped a soln. of HCl in Et2O, boiling for 4,5 h; filtration, concn. at 12 Torr, distn.; elem. anal.;
- Guidance literature:
-
In
neat (no solvent);
byproducts: C2H6; heating of the NH-1,2,5-azoniasilaboratole at 170-210°C for 3 h; distn.; elem. anal.;