1-Phenyl-2-(trimethylsilyl)aziridine

Base Information

• Chemical Name: 1-Phenyl-2-(trimethylsilyl)aziridine
• CAS No.: 128165-64-0
• Molecular Formula: C₁₁H₁₇NSi
• Molecular Weight: 191.348
• DSSTox Substance ID: DTXSID50568544
• Nikkaji Number: J437.275A
• Mol file: 128165-64-0.mol

Synonyms:1-Phenyl-2-(trimethylsilyl)aziridine;128165-64-0;DTXSID50568544

Chemical Property of 1-Phenyl-2-(trimethylsilyl)aziridine

Chemical Property:

• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 191.113026081
• Heavy Atom Count: 13
• Complexity: 179

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[Si](C)(C)C1CN1C2=CC=CC=C2

Technology Process of 1-Phenyl-2-(trimethylsilyl)aziridine

There total 3 articles about 1-Phenyl-2-(trimethylsilyl)aziridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

Phenyl azide (622-37-7) + ethenyltrimethylsilane (754-05-2) → 1-Phenyl-2-trimethylsilylaziridine (128165-64-0) + 3-(N-Anilinomethyl)-4,5-dihydro-3,5-bis(trimethylsilyl)-1H-pyrazole (138801-76-0)

Guidance literature:

In neat (no solvent); at 25 ℃; for 960h;

Reference yield: 61.2%

Phenyl azide (622-37-7) + ethenyltrimethylsilane (754-05-2) → 1-Phenyl-2-trimethylsilylaziridine (128165-64-0)

Guidance literature:

at 55 ℃; for 8h;

DOI:10.1039/a905182a

Reference yield:

Phenyl azide (622-37-7) + ethenyltrimethylsilane (754-05-2) → 1-Phenyl-2-trimethylsilylaziridine (128165-64-0) + 1-Phenyl-5-trimethylsilyl-1,2,3-triazoline

Guidance literature:

for 1h; Title compound not separated from byproducts.; UV-irradiation;

DOI:10.1039/a905182a

upstream raw materials:

Phenyl azide

ethenyltrimethylsilane

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