Technology Process of 2-(Benzyloxy)-3,3-dimethylbutanal
There total 16 articles about 2-(Benzyloxy)-3,3-dimethylbutanal which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: DMAP, Et3N / dimethylformamide / 48 h / Ambient temperature
2: 1.) NaH / 1.) THF, 24 h, 2.) THF, 2 d
3: TsOH / methanol / 8 h / 80 °C
4: 1.) oxalyl chloride, DMSO, 2.) Et3N / 1.) CH2Cl2, -78 deg C, 45 min, 2.)CH2Cl2, 0 deg C, overnight
With
dmap; oxalyl dichloride; sodium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine;
In
methanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) NaH / 1.) THF, 24 h, 2.) THF, 2 d
2: TsOH / methanol / 8 h / 80 °C
3: 1.) oxalyl chloride, DMSO, 2.) Et3N / 1.) CH2Cl2, -78 deg C, 45 min, 2.)CH2Cl2, 0 deg C, overnight
With
oxalyl dichloride; sodium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine;
In
methanol;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) NaH / 1.) THF, 24 h, 2.) THF, 2 d
2: TsOH / methanol / 8 h / 80 °C
3: 1.) oxalyl chloride, DMSO, 2.) Et3N / 1.) CH2Cl2, -78 deg C, 45 min, 2.)CH2Cl2, 0 deg C, overnight
With
oxalyl dichloride; sodium hydride; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine;
In
methanol;
