Benzoyl chloride, 2-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-

Base Information

Chemical Name:Benzoyl chloride, 2-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-
CAS No.:129452-86-4
Molecular Formula:C24H25ClO2Si
Molecular Weight:409
Hs Code.:
DSSTox Substance ID:DTXSID20464600
Wikidata:Q82289991

Synonyms:129452-86-4;Benzoyl chloride, 2-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-;SCHEMBL10349815;DTXSID20464600

Suppliers and Price of Benzoyl chloride, 2-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Benzoyl chloride, 2-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:7
Exact Mass:408.1312343
Heavy Atom Count:28
Complexity:485

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)[Si](C1=CC=CC=C1)(C2=CC=CC=C2)OCC3=CC=CC=C3C(=O)Cl

Technology Process of Benzoyl chloride, 2-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-

There total 9 articles about Benzoyl chloride, 2-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 132286-88-5
2-(((tert-butyldiphenylsilyl)oxy)methyl)benzoic acid

: 129452-86-4
2-<(tert-butyldiphenylsilyloxy)methyl>benzoyl chloride

Guidance literature:: With oxalyl dichloride; In toluene; at 50 ℃; for 1h;

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 129452-86-4
2-<(tert-butyldiphenylsilyloxy)methyl>benzoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

2: Mg / in Et₂O

3: oxalyl chloride / toluene

With oxalyl dichloride; magnesium; In toluene;
DOI:10.1016/S0040-4039(00)94573-8

Reference yield:

: 87-41-2
2-benzofuran-1(3H)-one

: 129452-86-4
2-<(tert-butyldiphenylsilyloxy)methyl>benzoyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: KOH / methanol; H₂O / 1.5 h / Heating

2: pyridine / 20 °C

3: aq. K₂CO₃ / tetrahydrofuran; methanol / 0.5 h

4: 100 percent / oxalyl chloride / toluene / 1 h / 50 °C

With pyridine; potassium hydroxide; oxalyl dichloride; potassium carbonate; In tetrahydrofuran; methanol; water; toluene;