Glycine, N-(diphenylmethylene)-, (1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl ester

Base Information

Chemical Name:Glycine, N-(diphenylmethylene)-, (1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl ester
CAS No.:130156-98-8
Molecular Formula:C25H31NO2
Molecular Weight:377.527
Hs Code.:

Synonyms:

Suppliers and Price of Glycine, N-(diphenylmethylene)-, (1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of Glycine, N-(diphenylmethylene)-, (1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl ester

Chemical Property:

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Glycine, N-(diphenylmethylene)-, (1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl ester

There total 3 articles about Glycine, N-(diphenylmethylene)-, (1R,2S,5R)-5-methyl-2-(1-methylethyl)cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.7%

: 1013-88-3
Benzophenone imine

: 63254-60-4,80655-94-3,120143-37-5
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-aminoacetate

: 130156-98-8
(1R,2S,5R)-menthyl-N-(diphenylmethylidene)-glycinate

Guidance literature:: In dichloromethane; at 20 ℃; for 16h;
DOI:10.1021/jo010864i

Reference yield:

: 2216-51-5
(-)-menthol

: 130156-98-8
(1R,2S,5R)-menthyl-N-(diphenylmethylidene)-glycinate

Guidance literature:: Multi-step reaction with 3 steps

1: 91.7 percent / DMAP; DCC / acetonitrile / 48 h / 20 °C

2: triluoroacetic acid / 1.5 h / 20 °C

3: 74.7 percent / CH₂Cl₂ / 16 h / 20 °C

With dmap; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; acetonitrile;
DOI:10.1021/jo010864i

Reference yield:

: 145280-11-1
(1R,2S,5R)-2-(1-methylethyl)-5-methylcyclohexyl 2-<(tert-butoxycarbonyl)amino>acetate

: 130156-98-8
(1R,2S,5R)-menthyl-N-(diphenylmethylidene)-glycinate

Guidance literature:: Multi-step reaction with 2 steps

1: triluoroacetic acid / 1.5 h / 20 °C

2: 74.7 percent / CH₂Cl₂ / 16 h / 20 °C

With trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jo010864i