(1S,3S)-3-acetyl-3,5,12-trihydroxy-10-methoxy-6,11-dioxo-1,2,3,4,6,11-hexahydrotetracen-1-yl 3-(3-cyanomorpholin-4-yl)-2,3,6-trideoxy-alpha-L-lyxo-hexopyranoside

Base Information

• Chemical Name: (1S,3S)-3-acetyl-3,5,12-trihydroxy-10-methoxy-6,11-dioxo-1,2,3,4,6,11-hexahydrotetracen-1-yl 3-(3-cyanomorpholin-4-yl)-2,3,6-trideoxy-alpha-L-lyxo-hexopyranoside
• CAS No.: 89196-06-5
• Molecular Formula: C₃₂H₃₄N₂O₁₁
• Molecular Weight: 622.629

Synonyms:

Chemical Property of (1S,3S)-3-acetyl-3,5,12-trihydroxy-10-methoxy-6,11-dioxo-1,2,3,4,6,11-hexahydrotetracen-1-yl 3-(3-cyanomorpholin-4-yl)-2,3,6-trideoxy-alpha-L-lyxo-hexopyranoside

Chemical Property:

• Vapor Pressure: 1.06E-31mmHg at 25°C
• Boiling Point: 862.2°C at 760 mmHg
• Flash Point: 475.2°C
• Density: 1.54g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of (1S,3S)-3-acetyl-3,5,12-trihydroxy-10-methoxy-6,11-dioxo-1,2,3,4,6,11-hexahydrotetracen-1-yl 3-(3-cyanomorpholin-4-yl)-2,3,6-trideoxy-alpha-L-lyxo-hexopyranoside

There total 2 articles about (1S,3S)-3-acetyl-3,5,12-trihydroxy-10-methoxy-6,11-dioxo-1,2,3,4,6,11-hexahydrotetracen-1-yl 3-(3-cyanomorpholin-4-yl)-2,3,6-trideoxy-alpha-L-lyxo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

2,2'-oxybis(acetaldehyde) (7456-83-9) + daunomycin hydrochloride (23541-50-6) → 3'-deamino-3'-morpholino-13,13-dihydrodaunorubicin (79867-79-1) + 3'-deamino-3'-morpholinodaunoribicin (79867-78-0,94730-46-8) + 3'-deamino-3'-(3-cyano-4-morpholinyl)-13-dihydrodaunorubicin (89164-75-0,89164-76-1,89617-37-8) + 3'-deamino-3'-(3-cyano-4-morpholinyl)daunorubicin (89617-36-7,89164-74-9,89196-06-5,94730-47-9)

Guidance literature:

With sodium cyanoborohydride; In water; acetonitrile;

DOI:10.1021/jm00371a014

Reference yield: 13.0%

2,2'-oxybis(acetaldehyde) (7456-83-9) + daunomycin hydrochloride (23541-50-6) + acetonitrile (75-05-8,26809-02-9) → 3'-deamino-3'-morpholino-13,13-dihydrodaunorubicin (79867-79-1) + 3'-deamino-3'-morpholinodaunoribicin (79867-78-0,94730-46-8) + 3'-deamino-3'-(3-cyano-4-morpholinyl)-13-dihydrodaunorubicin (89164-75-0,89164-76-1,89617-37-8) + 3'-deamino-3'-(3-cyano-4-morpholinyl)daunorubicin (89617-36-7,89164-74-9,89196-06-5,94730-47-9)

Guidance literature:

With citrate buffer; sodium cyanoborohydride; Yield given. Multistep reaction; 1.) H₂O;

DOI:10.1021/jm00371a014

upstream raw materials:

2,2'-oxybis(acetaldehyde)

daunomycin hydrochloride

acetonitrile

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