8-Quinolinol, 5-[(4-methoxyphenyl)azo]-

Base Information

Chemical Name:8-Quinolinol, 5-[(4-methoxyphenyl)azo]-
CAS No.:13071-14-2
Molecular Formula:C16H13N3O2
Molecular Weight:279.298
Hs Code.:
DSSTox Substance ID:DTXSID90425506
Nikkaji Number:J2.330.155E
ChEMBL ID:CHEMBL2094448,CHEMBL1447284,CHEMBL4553340

Synonyms:8-Quinolinol, 5-[(4-methoxyphenyl)azo]-;MLS000774606;SMR000372120;300572-27-4;13071-14-2;CHEMBL1447284;CHEMBL2094448;CHEMBL4553340;BDBM48098;cid_5924924;(5E)-5-[(4-methoxyphenyl)hydrazinylidene]quinolin-8-one;DTXSID90425506;HMS2764L05;DNDI1417101;STL306465;AKOS001028939;AKOS002346830;5-[(E)-(4-Methoxyphenyl)azo]quinoline-8-ol;5-[(E)-(4-methoxyphenyl)diazenyl]quinolin-8-ol;(5E)-5-[(4-methoxyphenyl)hydrazono]quinolin-8-one;Z56758742;(5E)-5-[(4-methoxyphenyl)hydrazinylidene]-8-quinolinone;(5Z)-5-[2-(4-methoxyphenyl)hydrazinylidene]quinolin-8(5H)-one

Suppliers and Price of 8-Quinolinol, 5-[(4-methoxyphenyl)azo]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 8-Quinolinol, 5-[(4-methoxyphenyl)azo]-

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:279.100776666
Heavy Atom Count:21
Complexity:355

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)N=NC2=C3C=CC=NC3=C(C=C2)O

Technology Process of 8-Quinolinol, 5-[(4-methoxyphenyl)azo]-

There total 1 articles about 8-Quinolinol, 5-[(4-methoxyphenyl)azo]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 148-24-3,24804-14-6
8-quinolinol

: 104-94-9
4-methoxy-aniline

: 13071-14-2
5-(2-(4-methoxyphenyl)diazenyl)quinolin-8-ol

Guidance literature:: With 3,5-dimethylpyridinium hydrogensulphate; sodium nitrite; In water; Reagent/catalyst; Solvent; Microwave irradiation;

Reference yield: 80.0%

: 7631-95-0
sodium molybdate dihydrate

: 13071-14-2
5-(2-(4-methoxyphenyl)diazenyl)quinolin-8-ol

: di-μ-oxo-bis(5-(p-methoxyphenylazo)-8-hydroxyquinolato)-oxomolybdenum(V)

Guidance literature:: With sodium hydroxide; sodium dithionite; In ethanol; water; treating a soln. of Na2MoO4*2H2O in water with concd. NaOH, addn. to a soln. of ligand in hot ethanol, addn. of a freshly prepared soln. of sodium dithionite in water; dropwise addn. of aq. HCl until pptn. is complete, filtn. by suction, drying in vacuo over P4O10, elem. anal.;

Reference yield: 65.0%

: 7631-95-0
sodium molybdate dihydrate

: 1015-38-9
diphenylphosphinodithioic acid

: 13071-14-2
5-(2-(4-methoxyphenyl)diazenyl)quinolin-8-ol

: di-μ-oxo-(5-(p-methoxyphenylazo)-8-hydroxyquinolato)(diphenyldithiophosphinato)-oxomolybdenum(V)

Guidance literature:: With sodium hydroxide; In methanol; ethanol; water; treating a soln. of Na2MoO4*2H2O in water with concd. NaOH till reaching pH 10, addn. to a soln. of ligand in ethanol, addn. of a soln. of diphenyldithiophospinic acid in MeOH at 0-5°C with continuous stirring, stirring for 1 h at the same temp.; filtn., washing with MeOH, drying over P4O10, elem. anal.;