2-Hepten-1-ol, 7-[(4-methoxyphenyl)methoxy]-, (2E)-

Base Information

Chemical Name:2-Hepten-1-ol, 7-[(4-methoxyphenyl)methoxy]-, (2E)-
CAS No.:131375-65-0
Molecular Formula:C15H22O3
Molecular Weight:250.338
Hs Code.:

Synonyms:

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Chemical Property of 2-Hepten-1-ol, 7-[(4-methoxyphenyl)methoxy]-, (2E)-

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Technology Process of 2-Hepten-1-ol, 7-[(4-methoxyphenyl)methoxy]-, (2E)-

There total 13 articles about 2-Hepten-1-ol, 7-[(4-methoxyphenyl)methoxy]-, (2E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 131375-64-9
ethyl 7-(4-methoxyphenylmethoxy)-hept-2-enoate

: 131375-65-0
7-(4-methoxyphenylmethoxy)-hept-2-en-1-ol

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; cyclohexane; at -78 ℃; for 0.333333h;
DOI:10.1021/ol051415y

Reference yield: 98.0%

: methyl (E)-7-(4-methoxybenzyloxy)hept-2-enoate

: 131375-65-0
7-(4-methoxyphenylmethoxy)-hept-2-en-1-ol

Guidance literature:: methyl (E)-7-(4-methoxybenzyloxy)hept-2-enoate; With diisobutylaluminium hydride; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 4h; Inert atmosphere;

With methanol; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1039/c7ob00079k

Reference yield:

: 131375-63-8
5-(4-methoxybenzyloxy)-1-pentanol

: 131375-65-0
7-(4-methoxyphenylmethoxy)-hept-2-en-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: 100 percent / oxalyl chloride; DMSO; triethylamine / CH₂Cl₂ / -78 - 22 °C

2.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C

2.2: 91 percent / tetrahydrofuran / 0.33 h / 22 °C

3.1: 100 percent / diisobutylaluminum hydride / cyclohexane; CH₂Cl₂ / 0.33 h / -78 °C

With oxalyl dichloride; sodium hydride; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane; cyclohexane; 1.1: Swern oxidation / 2.2: Horner-Emmons reaction;
DOI:10.1021/ol051415y