1-Phenyl-3-pyridin-3-ylthiourea

Base Information

Chemical Name:1-Phenyl-3-pyridin-3-ylthiourea
CAS No.:13140-69-7
Molecular Formula:C12H11N3S
Molecular Weight:229.305
Hs Code.:
ChEMBL ID:CHEMBL3120552
DSSTox Substance ID:DTXSID00409413
Nikkaji Number:J1.227.646J
Wikidata:Q82215241

Synonyms:CHEMBL3120552;1-phenyl-3-pyridin-3-ylthiourea;13140-69-7;Oprea1_602028;SCHEMBL11186307;DTXSID00409413;N-(3-pyridyl)-N'-phenylthiourea;BDBM50448175;AKOS002806470;N-PHENYL-N'-(3-PYRIDYL)THIOUREA;3-PHENYL-1-(PYRIDIN-3-YL)THIOUREA;EN300-10181849;Z45796210

Suppliers and Price of 1-Phenyl-3-pyridin-3-ylthiourea

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1-Phenyl-3-pyridin-3-ylthiourea

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:229.06736854
Heavy Atom Count:16
Complexity:226

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)NC(=S)NC2=CN=CC=C2

Technology Process of 1-Phenyl-3-pyridin-3-ylthiourea

There total 1 articles about 1-Phenyl-3-pyridin-3-ylthiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.9%

: 462-08-8
pyridin-3-ylamine

: 103-72-0
phenyl isothiocyanate

: 13140-69-7
1-phenyl-3-(pyridin-3-yl)thiourea

Guidance literature:: In ethanol;
DOI:10.1007/s10870-007-9246-1

Reference yield: 90.4%

: 3251-29-4
cuprous nitrate

: 13140-69-7
1-phenyl-3-(pyridin-3-yl)thiourea

: 75-05-8,26809-02-9
acetonitrile

: CuNO₃(N-(3-pyridyl)-N'-phenylthiourea)*MeCN

Guidance literature:: In acetonitrile; to soln. of CuNO3 (prepd. in situ) proper thiourea ligand added as a solid, suspn. stirred for 1 h at room temp. under N2; solid filtered off, washed (Et2O), dried (vac.); elem.anal.;
DOI:10.1016/j.poly.2009.08.023

Reference yield: 87.7%

: 13140-69-7
1-phenyl-3-(pyridin-3-yl)thiourea

: 7787-70-4
copper(I) bromide

: CuBr(N-(3-pyridyl)-N'-phenylthiourea)2

Guidance literature:: In acetonitrile; CuBr dissolved in MeCN under N2, then proper thiourea ligand added as a solid, suspn. stirred for 1 h at room temp. under N2; solid filtered off, washed (Et2O), dried (vac.); elem.anal.;
DOI:10.1016/j.poly.2009.08.023