Technology Process of Triacontanoic acid, 30-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-,
4-nitrophenyl ester
There total 9 articles about Triacontanoic acid, 30-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-,
4-nitrophenyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine;
for 1.5h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 12.3 g / p-TsOH / 24 h / Heating
2: pyridinium chlorochromate, 4A molecular sieves / CH2Cl2 / 0.33 h / Ambient temperature
4: 90 percent / H2 / 10percent Pd/C / ethyl acetate / 24 h / Ambient temperature
5: 86 percent / 85.5percent KOH / aq. ethanol / 2.5 h / 60 °C
6: 95 percent / pyridine / 1.5 h / Ambient temperature
With
pyridine; potassium hydroxide; 4 A molecular sieve; hydrogen; toluene-4-sulfonic acid; pyridinium chlorochromate;
palladium on activated charcoal;
In
ethanol; dichloromethane; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: pyridinium chlorochromate, 4A molecular sieves / CH2Cl2 / 0.33 h / Ambient temperature
3: 90 percent / H2 / 10percent Pd/C / ethyl acetate / 24 h / Ambient temperature
4: 86 percent / 85.5percent KOH / aq. ethanol / 2.5 h / 60 °C
5: 95 percent / pyridine / 1.5 h / Ambient temperature
With
pyridine; potassium hydroxide; 4 A molecular sieve; hydrogen; pyridinium chlorochromate;
palladium on activated charcoal;
In
ethanol; dichloromethane; ethyl acetate;
