Technology Process of 4-Nitrophenyl 30-hydroxytriacontanoate
There total 11 articles about 4-Nitrophenyl 30-hydroxytriacontanoate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
boron trifluoride diethyl etherate;
In
chloroform;
for 28h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 12.3 g / p-TsOH / 24 h / Heating
2: pyridinium chlorochromate, 4A molecular sieves / CH2Cl2 / 0.33 h / Ambient temperature
4: 90 percent / H2 / 10percent Pd/C / ethyl acetate / 24 h / Ambient temperature
5: 86 percent / 85.5percent KOH / aq. ethanol / 2.5 h / 60 °C
6: 95 percent / pyridine / 1.5 h / Ambient temperature
7: 88 percent / BF3*Et2O / CHCl3 / 28 h / Ambient temperature
With
pyridine; potassium hydroxide; 4 A molecular sieve; boron trifluoride diethyl etherate; hydrogen; toluene-4-sulfonic acid; pyridinium chlorochromate;
palladium on activated charcoal;
In
ethanol; dichloromethane; chloroform; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: pyridinium chlorochromate, 4A molecular sieves / CH2Cl2 / 0.33 h / Ambient temperature
3: 90 percent / H2 / 10percent Pd/C / ethyl acetate / 24 h / Ambient temperature
4: 86 percent / 85.5percent KOH / aq. ethanol / 2.5 h / 60 °C
5: 95 percent / pyridine / 1.5 h / Ambient temperature
6: 88 percent / BF3*Et2O / CHCl3 / 28 h / Ambient temperature
With
pyridine; potassium hydroxide; 4 A molecular sieve; boron trifluoride diethyl etherate; hydrogen; pyridinium chlorochromate;
palladium on activated charcoal;
In
ethanol; dichloromethane; chloroform; ethyl acetate;
