Bicyclo[3.2.1]oct-3-ene-6-acetic acid, 3-(phenylmethyl)-, 2-hydroxyethyl ester, endo-

Base Information

Chemical Name:Bicyclo[3.2.1]oct-3-ene-6-acetic acid, 3-(phenylmethyl)-, 2-hydroxyethyl ester, endo-
CAS No.:133383-96-7
Molecular Formula:C₁₉H₂₄O₃
Molecular Weight:300.398
Hs Code.:

Synonyms:

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Chemical Property of Bicyclo[3.2.1]oct-3-ene-6-acetic acid, 3-(phenylmethyl)-, 2-hydroxyethyl ester, endo-

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Technology Process of Bicyclo[3.2.1]oct-3-ene-6-acetic acid, 3-(phenylmethyl)-, 2-hydroxyethyl ester, endo-

There total 9 articles about Bicyclo[3.2.1]oct-3-ene-6-acetic acid, 3-(phenylmethyl)-, 2-hydroxyethyl ester, endo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 133383-92-3
7α-(2-oxo-3-phenylpropyl)-1βH,5βH-bicyclo<3.3.0>octane-3-one

: 107-21-1
ethylene glycol

: 133383-96-7
((1R,5R,6R)-3-Benzyl-bicyclo[3.2.1]oct-3-en-6-yl)-acetic acid 2-hydroxy-ethyl ester

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; Ambient temperature; 1-2 h;
DOI:10.1016/S0040-4020(01)81224-2

Reference yield:

: 99524-57-9
C₁₃H₁₈O₄

: 133383-96-7
((1R,5R,6R)-3-Benzyl-bicyclo[3.2.1]oct-3-en-6-yl)-acetic acid 2-hydroxy-ethyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: H₂ / 5percent Pd/C / methanol

2: LiAlH₄ / diethyl ether

3: PDC / CH₂Cl₂

4: tetrahydrofuran

5: PCC / CH₂Cl₂

6: 3percent aq. H₂SO₄ / acetone

7: 10 percent / BF₃-etherate / CH₂Cl₂ / Ambient temperature; 1-2 h

With lithium aluminium tetrahydride; dipyridinium dichromate; sulfuric acid; boron trifluoride diethyl etherate; hydrogen; pyridinium chlorochromate; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; acetone;
DOI:10.1016/S0040-4020(01)81224-2

Reference yield:

: 766-04-1
benzyllithium

: 133383-96-7
((1R,5R,6R)-3-Benzyl-bicyclo[3.2.1]oct-3-en-6-yl)-acetic acid 2-hydroxy-ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran

2: PCC / CH₂Cl₂

3: 3percent aq. H₂SO₄ / acetone

4: 10 percent / BF₃-etherate / CH₂Cl₂ / Ambient temperature; 1-2 h

With sulfuric acid; boron trifluoride diethyl etherate; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1016/S0040-4020(01)81224-2