1-Decanone, 1-(6-hydroxy-2,3,4-trimethoxyphenyl)-

Base Information

Chemical Name:1-Decanone, 1-(6-hydroxy-2,3,4-trimethoxyphenyl)-
CAS No.:134081-72-4
Molecular Formula:C19H30O5
Molecular Weight:338.444
Hs Code.:

Synonyms:

Suppliers and Price of 1-Decanone, 1-(6-hydroxy-2,3,4-trimethoxyphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-Decanone, 1-(6-hydroxy-2,3,4-trimethoxyphenyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-Decanone, 1-(6-hydroxy-2,3,4-trimethoxyphenyl)-

There total 10 articles about 1-Decanone, 1-(6-hydroxy-2,3,4-trimethoxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-(6-Benzyloxy-2,3,4-trimethoxy-phenyl)-decan-1-one

: 134081-72-4
1-(6-Hydroxy-2,3,4-trimethoxy-phenyl)-decan-1-one

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; ethyl acetate; Yield given;
DOI:10.1021/jm00111a037

Reference yield:

: 5333-45-9
1,2,3,5-tetramethoxybenzene

: 134081-72-4
1-(6-Hydroxy-2,3,4-trimethoxy-phenyl)-decan-1-one

Guidance literature:: Multi-step reaction with 9 steps

1: aluminum chloride / diethyl ether / 0.5 h / 0 °C

2: aluminum chloride / acetonitrile / 2 h / 50 °C

3: 83 percent / potassium carbonate / acetone / Heating

4: 90 percent / aluminum bromide / acetonitrile / 3 h / Ambient temperature

5: 83 percent / potassium carbonate / methanol / Heating

6: potassium carbonate / dimethylformamide / 0.33 h / 150 - 160 °C

7: concd. hydrochloric acid, acetic acid / 3 h / Ambient temperature

8: potassium carbonate / acetone / Heating

9: H₂ / 10percent Pd/C / ethyl acetate; methanol

With hydrogenchloride; aluminium trichloride; aluminum tri-bromide; hydrogen; potassium carbonate; acetic acid; palladium on activated charcoal; In methanol; diethyl ether; ethyl acetate; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1021/jm00111a037

Reference yield:

: 134081-96-2
1-(2,6-Dihydroxy-3,4-dimethoxy-phenyl)-decan-1-one

: 134081-72-4
1-(6-Hydroxy-2,3,4-trimethoxy-phenyl)-decan-1-one

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / dimethylformamide / 0.33 h / 150 - 160 °C

2: concd. hydrochloric acid, acetic acid / 3 h / Ambient temperature

3: potassium carbonate / acetone / Heating

4: H₂ / 10percent Pd/C / ethyl acetate; methanol

With hydrogenchloride; hydrogen; potassium carbonate; acetic acid; palladium on activated charcoal; In methanol; ethyl acetate; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm00111a037