3-Buten-2-one, 3-(phenylthio)-

Base Information

Chemical Name:3-Buten-2-one, 3-(phenylthio)-
CAS No.:13522-48-0
Molecular Formula:C10H10OS
Molecular Weight:178.255
Hs Code.:
DSSTox Substance ID:DTXSID20506610
Wikidata:Q82362445
Mol file:13522-48-0.mol

Synonyms:13522-48-0;3-(Phenylsulfanyl)but-3-en-2-one;methyl 1-phenylthiovinyl ketone;DTXSID20506610

Suppliers and Price of 3-Buten-2-one, 3-(phenylthio)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3-Buten-2-one, 3-(phenylthio)-

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:178.04523611
Heavy Atom Count:12
Complexity:180

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)C(=C)SC1=CC=CC=C1

Technology Process of 3-Buten-2-one, 3-(phenylthio)-

There total 23 articles about 3-Buten-2-one, 3-(phenylthio)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 33487-46-6
3-chloro-3-phenylthio-2-butanone

: 13522-48-0
3-(phenylthio)-but-3-en-2-one

Guidance literature:: With pyridine; In toluene; at 200 ℃; pyrolysis in a glass column filled with glass wool;
DOI:10.1016/S0040-4039(00)85565-3

Reference yield: 52.0%

: 77202-27-8
3-(phenylthio)-3-buten-2-ol

: 13522-48-0
3-(phenylthio)-but-3-en-2-one

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In benzene; at 0 ℃; for 24h;
DOI:10.1021/jo00346a012

Reference yield:

: 60603-14-7
(±)-2-(phenylthio)cyclobutanone

: 13522-48-0
3-(phenylthio)-but-3-en-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: KH / tetrahydrofuran; dimethylformamide

2: hexane / 340 °C

3: (hydrolysis)

With potassium hydride; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;
DOI:10.1021/ja00432a055