Octanoic acid, 8-bromo-, 2-oxo-1,2-diphenylethyl ester

Base Information

Chemical Name:Octanoic acid, 8-bromo-, 2-oxo-1,2-diphenylethyl ester
CAS No.:136451-84-8
Molecular Formula:C22H25BrO3
Molecular Weight:417.343
Hs Code.:

Synonyms:

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Chemical Property of Octanoic acid, 8-bromo-, 2-oxo-1,2-diphenylethyl ester

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Technology Process of Octanoic acid, 8-bromo-, 2-oxo-1,2-diphenylethyl ester

There total 1 articles about Octanoic acid, 8-bromo-, 2-oxo-1,2-diphenylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 17696-11-6
8-bromooctanoic acid

: 119-53-9,579-44-2
2-hydroxy-2-phenylacetophenone

: 136451-84-8
2-oxo-1,2-diphenylethyl 8-bromooctanoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 17h; Ambient temperature;
DOI:10.1021/jm00097a006

Reference yield: 86.0%

: 136451-84-8
2-oxo-1,2-diphenylethyl 8-bromooctanoate

: 136451-85-9
2-(7-bromoheptyl)-4,5-diphenyloxazole

Guidance literature:: With ammonium acetate; In acetic acid; for 1h; Heating;
DOI:10.1021/jm00097a006

Reference yield:

: 136451-84-8
2-oxo-1,2-diphenylethyl 8-bromooctanoate

: 136451-87-1
2-[7-(4,5-diphenyl-2-oxazolyl)heptyl]propanedioic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / NH₄OAc / acetic acid / 1 h / Heating

2: 83 percent / potassium tert-butoxide, 18-crown-6 / tetrahydrofuran / 17.5 h / Heating

3: 100 percent / aq. 5N NaOH / methanol / 1.) RT, 10 min, 2.) reflux, 4 h

With sodium hydroxide; 18-crown-6 ether; potassium tert-butylate; ammonium acetate; In tetrahydrofuran; methanol; acetic acid;
DOI:10.1021/jm00097a006