3-Azi-1-methoxybutylgalactopyranoside

Base Information

Chemical Name:3-Azi-1-methoxybutylgalactopyranoside
CAS No.:117405-74-0
Molecular Formula:C₁₁H₂₀N₂O₇
Molecular Weight:292.289
Hs Code.:
DSSTox Substance ID:DTXSID30151776
Mol file:117405-74-0.mol

Synonyms:3-AMBGP;3-azi-1-methoxybutyl-beta-D-galactopyranoside;3-azi-1-methoxybutylgalactopyranoside

Suppliers and Price of 3-Azi-1-methoxybutylgalactopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 3-Azi-1-methoxybutylgalactopyranoside

Chemical Property:

Vapor Pressure:1.29E-09mmHg at 25°C
Boiling Point:440.6°Cat760mmHg
Flash Point:220.3°C
PSA：133.33000
Density:1.58g/cm³
LogP:-2.77970
XLogP3:-1.8
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:9
Rotatable Bond Count:5
Exact Mass:292.12705098
Heavy Atom Count:20
Complexity:400

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC1(C(C(C(C(O1)CO)O)O)(C2(N=N2)C)O)OC
Isomeric SMILES:CCO[C@]1([C@]([C@H]([C@H]([C@H](O1)CO)O)O)(C2(N=N2)C)O)OC

Technology Process of 3-Azi-1-methoxybutylgalactopyranoside

There total 1 articles about 3-Azi-1-methoxybutylgalactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 98807-67-1,98807-69-3,104757-96-2,104757-97-3,117405-71-7,117405-72-8
3-azi-1-methoxybutyl 2,3,4,6-tetra-O-acetyl-β-D-galactopyranoside

: 94885-16-2,98856-35-0,98856-36-1,105088-21-9,105088-22-0,105088-29-7,117405-74-0,117405-77-3
3-azi-1-methoxybutyl β-D-galactopyranoside

Guidance literature:: With sodium methylate; for 0.5h;
DOI:10.1016/0008-6215(88)85083-3

Reference yield:

: 94885-16-2,98856-35-0,98856-36-1,105088-21-9,105088-22-0,105088-29-7,117405-74-0,117405-77-3
3-azi-1-methoxybutyl β-D-galactopyranoside

: 3-azi-1-methoxybutyl O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1<*>6)-2,3,4-tri-O-benzoyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) pyridine, 2.) pyridine, 4-(dimethylamino)pyridine / 1.) THF, RT, 3 h, 2.) THF, RT

2: 54 percent / CH₂Cl₂ / 192 h / -78 °C

With pyridine; dmap; In dichloromethane;
DOI:10.1021/jo00287a026