9-Methyl-1,2,3,4,6,7,12,12b-octahydroindolo(2,3-a)quinolizine

Base Information

Chemical Name:9-Methyl-1,2,3,4,6,7,12,12b-octahydroindolo(2,3-a)quinolizine
CAS No.:16008-64-3
Molecular Formula:C₁₆H₂₀N₂
Molecular Weight:240.348
Hs Code.:2933990090
DSSTox Substance ID:DTXSID20936216
Nikkaji Number:J691.170F
Mol file:16008-64-3.mol

Synonyms:9-methyl-1,2,3,4,6,7,12,12b-octahydroindolo(2,3-a)quinolizine;9-methyl-1,2,3,4,6,7,12,12b-octahydroindolo(2,3-a)quinolizine hydrochloride;MIQ compound

Suppliers and Price of 9-Methyl-1,2,3,4,6,7,12,12b-octahydroindolo(2,3-a)quinolizine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
9-METHYL-1,2,3,4,6,7,12,12B-OCTAHYDROINDOLO(2,3-A)QUINOLIZINE 95.00%
5MG
$ 497.35

Total 3 raw suppliers

Chemical Property of 9-Methyl-1,2,3,4,6,7,12,12b-octahydroindolo(2,3-a)quinolizine

Chemical Property:

Vapor Pressure:5.76E-07mmHg at 25°C
Melting Point:141-142 °C
Boiling Point:411°Cat760mmHg
PKA:18.49±0.20(Predicted)
Flash Point:202.4°C
PSA：19.03000
Density:1.18g/cm³
LogP:3.49730
XLogP3:3.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:240.162648646
Heavy Atom Count:18
Complexity:316

Purity/Quality:

99% ^*data from raw suppliers

9-METHYL-1,2,3,4,6,7,12,12B-OCTAHYDROINDOLO(2,3-A)QUINOLIZINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC2=C(C=C1)NC3=C2CCN4C3CCCC4

Technology Process of 9-Methyl-1,2,3,4,6,7,12,12b-octahydroindolo(2,3-a)quinolizine

There total 4 articles about 9-Methyl-1,2,3,4,6,7,12,12b-octahydroindolo(2,3-a)quinolizine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: N-[Hexahydro-quinolizin-(1E)-ylidene]-N'-(4-methyl-cyclohexa-2,4-dienyl)-hydrazine

: 16008-64-3
9-methyl-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizine

Guidance literature:: With hydrogenchloride; In ethanol; for 4h; Heating;

Reference yield: 12.0%

: 10447-21-9
hexahydro-quinolizin-1-one

: 539-44-6
N-4-methylphenylhydrazine

: 16008-64-3
9-methyl-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizine

: 134504-12-4
(3,4,6,7,8,9-Hexahydro-2H-quinolizin-1-yl)-p-tolyl-diazene

Guidance literature:: With hydrogenchloride; phosphoric acid; In ethanol; for 3.5h; Heating; or with the appropriate hydrazine*HCl;

Reference yield:

: 10447-21-9
hexahydro-quinolizin-1-one

: 16008-64-3
9-methyl-1,2,3,4,6,7,12,12b-octahydro-indolo[2,3-a]quinolizine

Guidance literature:: Multi-step reaction with 2 steps

1: 0.5 h / 100 °C

2: 55 percent / HCl / ethanol / 4 h / Heating

With hydrogenchloride; In ethanol;